C₂₄H₁₃ClF₅NO₄

Base Information

Chemical Name:C₂₄H₁₃ClF₅NO₄
CAS No.:1364740-36-2
Molecular Formula:C₂₄H₁₃ClF₅NO₄
Molecular Weight:509.817
Hs Code.:

C<sub>24</sub>H<sub>13</sub>ClF<sub>5</sub>NO<sub>4</sub>

Synonyms:

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Chemical Property of C₂₄H₁₃ClF₅NO₄

Chemical Property:

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Technology Process of C₂₄H₁₃ClF₅NO₄

There total 20 articles about C₂₄H₁₃ClF₅NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 443-86-7
3-fluoro-2-methylaniline

: 4-{2-[4-chloro-2-(3-fluoro-5-trifluoromethylbenzoyl)phenoxy]acetylamino}-2-fluoro-3-methylbenzoic acid

: 1364740-54-4
C₂₂H₁₃ClF₅NO₃

: 1364740-36-2
C₂₄H₁₃ClF₅NO₄

Guidance literature:: Multi-step reaction with 3 steps

1: sodium perborate; potassium iodide / water; acetic acid / 1.5 h / 5 - 20 °C

2: para-methylphenylmagnesium bromide / tetrahydrofuran

3: potassium phosphate / acetonitrile / 10.5 h / 0 - 20 °C

With sodium perborate; potassium phosphate; para-methylphenylmagnesium bromide; potassium iodide; In tetrahydrofuran; water; acetic acid; acetonitrile;
DOI:10.1021/op200301h

Reference yield:

: 194804-84-7
2-fluoro-3-methyl-4-aminobenzoic acid

: 675139-67-0
[4-chloro-2-(3-fluoro-5-trifluoromethylbenzoyl)phenoxy]acetyl chloride

: 4-{2-[4-chloro-2-(3-fluoro-5-trifluoromethylbenzoyl)phenoxy]acetylamino}-2-fluoro-3-methylbenzoic acid

: 1364740-54-4
C₂₂H₁₃ClF₅NO₃

: 1364740-36-2
C₂₄H₁₃ClF₅NO₄

Guidance literature:: With potassium phosphate; In acetonitrile; at 0 - 20 ℃; for 10.5h;
DOI:10.1021/op200301h

Reference yield:

: 329927-16-4
2-fluoro-3-methyl-4-aminophenyl iodide

: 4-{2-[4-chloro-2-(3-fluoro-5-trifluoromethylbenzoyl)phenoxy]acetylamino}-2-fluoro-3-methylbenzoic acid

: 1364740-54-4
C₂₂H₁₃ClF₅NO₃

: 1364740-36-2
C₂₄H₁₃ClF₅NO₄

Guidance literature:: Multi-step reaction with 2 steps

1: para-methylphenylmagnesium bromide / tetrahydrofuran

2: potassium phosphate / acetonitrile / 10.5 h / 0 - 20 °C

With potassium phosphate; para-methylphenylmagnesium bromide; In tetrahydrofuran; acetonitrile;
DOI:10.1021/op200301h