C₁₅H₁₈BrNO₂

Base Information

Chemical Name:C₁₅H₁₈BrNO₂
CAS No.:1389321-66-7
Molecular Formula:C₁₅H₁₈BrNO₂
Molecular Weight:324.217
Hs Code.:

C<sub>15</sub>H<sub>18</sub>BrNO<sub>2</sub>

Synonyms:

Suppliers and Price of C₁₅H₁₈BrNO₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₁₈BrNO₂

Chemical Property:

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Technology Process of C₁₅H₁₈BrNO₂

There total 11 articles about C₁₅H₁₈BrNO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: C₁₇H₂₂BrNO₂

: 1389321-66-7
C₁₅H₁₈BrNO₂

Guidance literature:: With Hoveyda-Grubbs catalyst second generation; In dichloromethane; for 24h; Inert atmosphere; Reflux;
DOI:10.1055/s-0031-1291047

Reference yield:

: C₉H₈Br₂O₂

: 1389321-66-7
C₁₅H₁₈BrNO₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: boron trifluoride diethyl etherate / tetrahydrofuran / 1 h / 20 °C

2.1: titanium tetrachloride / dichloromethane / 0.17 h / 0 °C

2.2: 0.5 h / 0 °C

2.3: 3.5 h / -78 - 0 °C

3.1: 1H-imidazole / dichloromethane / 24 h / 20 °C

4.1: 1H-imidazole / N,N-dimethyl-formamide / 24 h / 20 °C

5.1: tetrahydrofuran / 0 °C

6.1: n-butyllithium / tetrahydrofuran; hexane / 0.58 h / 0 - 20 °C

6.2: 0 - 20 °C

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 24 h / 20 °C

8.1: di-isopropyl azodicarboxylate; diphenyl phosphoryl azide; triphenylphosphine / tetrahydrofuran / 12 h / 0 °C

9.1: water; triphenylphosphine / tetrahydrofuran / 12 h / 45 °C

10.1: triethylamine / dichloromethane / 3 h / 0 - 20 °C

11.1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 24 h / Inert atmosphere; Reflux

With 1H-imidazole; n-butyllithium; Hoveyda-Grubbs catalyst second generation; di-isopropyl azodicarboxylate; diphenyl phosphoryl azide; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; water; titanium tetrachloride; triethylamine; triphenylphosphine; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; 2.3: Evans syn aldol reaction / 6.2: Wittig reaction / 9.1: Staudinger reaction;
DOI:10.1055/s-0031-1291047

Reference yield:

: 1183778-97-3
2-bromo-1-(2-bromo-4-methoxyphenyl)ethan-1-one

: 1389321-66-7
C₁₅H₁₈BrNO₂

Guidance literature:: Multi-step reaction with 12 steps

1.1: sodium tetrahydroborate / methanol / 0.5 h / 0 °C

1.2: 3 h / 20 °C

2.1: boron trifluoride diethyl etherate / tetrahydrofuran / 1 h / 20 °C

3.1: titanium tetrachloride / dichloromethane / 0.17 h / 0 °C

3.2: 0.5 h / 0 °C

3.3: 3.5 h / -78 - 0 °C

4.1: 1H-imidazole / dichloromethane / 24 h / 20 °C

5.1: 1H-imidazole / N,N-dimethyl-formamide / 24 h / 20 °C

6.1: tetrahydrofuran / 0 °C

7.1: n-butyllithium / tetrahydrofuran; hexane / 0.58 h / 0 - 20 °C

7.2: 0 - 20 °C

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 24 h / 20 °C

9.1: di-isopropyl azodicarboxylate; diphenyl phosphoryl azide; triphenylphosphine / tetrahydrofuran / 12 h / 0 °C

10.1: water; triphenylphosphine / tetrahydrofuran / 12 h / 45 °C

11.1: triethylamine / dichloromethane / 3 h / 0 - 20 °C

12.1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 24 h / Inert atmosphere; Reflux

With 1H-imidazole; sodium tetrahydroborate; n-butyllithium; Hoveyda-Grubbs catalyst second generation; di-isopropyl azodicarboxylate; diphenyl phosphoryl azide; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; water; titanium tetrachloride; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; hexane; dichloromethane; N,N-dimethyl-formamide; 3.3: Evans syn aldol reaction / 7.2: Wittig reaction / 10.1: Staudinger reaction;
DOI:10.1055/s-0031-1291047