(S)-methyl 2-(3,4-diaminobenzamido)-5-guanidinopentanoate

Base Information

Chemical Name:(S)-methyl 2-(3,4-diaminobenzamido)-5-guanidinopentanoate
CAS No.:1295565-41-1
Molecular Formula:C₁₄H₂₂N₆O₃
Molecular Weight:322.367
Hs Code.:

Synonyms:

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Chemical Property of (S)-methyl 2-(3,4-diaminobenzamido)-5-guanidinopentanoate

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Technology Process of (S)-methyl 2-(3,4-diaminobenzamido)-5-guanidinopentanoate

There total 4 articles about (S)-methyl 2-(3,4-diaminobenzamido)-5-guanidinopentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₃₀N₆O₅

: 1295565-41-1
(S)-methyl 2-(3,4-diaminobenzamido)-5-guanidinopentanoate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/jm501867s

Reference yield:

: 1298108-48-1
methyl 4-amino-3-((tert-butoxycarbonyl)amino)benzoate

: 1295565-41-1
(S)-methyl 2-(3,4-diaminobenzamido)-5-guanidinopentanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium hydroxide / 1,4-dioxane; water / 20 °C / Inert atmosphere

1.2: pH 2 / Inert atmosphere

2.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

3.1: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; lithium hydroxide; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm501867s

Reference yield:

: 36692-49-6
Methyl 3,4-diaminobenzoate

: 1295565-41-1
(S)-methyl 2-(3,4-diaminobenzamido)-5-guanidinopentanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: guanidine hydrochloride / ethanol / 0.67 h / 45 °C / Inert atmosphere

2.1: lithium hydroxide / 1,4-dioxane; water / 20 °C / Inert atmosphere

2.2: pH 2 / Inert atmosphere

3.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

4.1: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere

With guanidine hydrochloride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; lithium hydroxide; In 1,4-dioxane; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm501867s