4-cyanophenyl trans-4-(4,4,4-trifluorobutyl)cyclohexanecarboxylate

Base Information

Chemical Name:4-cyanophenyl trans-4-(4,4,4-trifluorobutyl)cyclohexanecarboxylate
CAS No.:104958-62-5
Molecular Formula:C₁₈H₂₀F₃NO₂
Molecular Weight:339.358
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-cyanophenyl trans-4-(4,4,4-trifluorobutyl)cyclohexanecarboxylate

Chemical Property:

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Technology Process of 4-cyanophenyl trans-4-(4,4,4-trifluorobutyl)cyclohexanecarboxylate

There total 8 articles about 4-cyanophenyl trans-4-(4,4,4-trifluorobutyl)cyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103945-68-2
4-n-(4,4,4-trifluorobutyl)benzoic acid

: 104958-62-5
4-cyanophenyl trans-4-(4,4,4-trifluorobutyl)cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / 94percent H₂SO₄ / 3 h / Heating

2: 87 percent / hydrogen / platinium black / acetic acid / 10 h / 20 - 25 °C / 36.8 Torr

3: 64 percent / 35percent HCl / acetic acid / 10 h / 160 °C / heated on a sealed tube

4: thionyl chloride / pyridine / Heating

5: pyridine

With hydrogenchloride; thionyl chloride; sulfuric acid; hydrogen; pyridine; platinum; In pyridine; acetic acid;

Reference yield:

: 104958-56-7
trans-e,e-4-(4,4,4-trifluorobutyl)cyclohexanecarboxylic acid

: 104958-62-5
4-cyanophenyl trans-4-(4,4,4-trifluorobutyl)cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / pyridine / Heating

2: pyridine

With thionyl chloride; pyridine; In pyridine;

Reference yield:

: 104958-59-0
methyl 4-(4,4,4-trifluorobutyl)benzoate

: 104958-62-5
4-cyanophenyl trans-4-(4,4,4-trifluorobutyl)cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / hydrogen / platinium black / acetic acid / 10 h / 20 - 25 °C / 36.8 Torr

2: 64 percent / 35percent HCl / acetic acid / 10 h / 160 °C / heated on a sealed tube

3: thionyl chloride / pyridine / Heating

4: pyridine

With hydrogenchloride; thionyl chloride; hydrogen; pyridine; platinum; In pyridine; acetic acid;