C₂₄H₄₃N₃O₁₃S₂*C₇H₈O₃S

Base Information

• Chemical Name: C₂₄H₄₃N₃O₁₃S₂*C₇H₈O₃S
• CAS No.: 1415712-86-5
• Molecular Formula: C₇H₈O₃S*C₂₄H₄₃N₃O₁₃S₂
• Molecular Weight: 817.954
• Mol file: 1415712-86-5.mol

Synonyms:

Chemical Property of C₂₄H₄₃N₃O₁₃S₂*C₇H₈O₃S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₄₃N₃O₁₃S₂*C₇H₈O₃S

There total 6 articles about C₂₄H₄₃N₃O₁₃S₂*C₇H₈O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C32H49N3O13S2 (1415712-80-9) → C24H43N3O13S2*C7H8O3S (1415712-86-5)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium permanganate / water; acetic acid / 1 h / -15 - -10 °C / Inert atmosphere

2: palladium on activated charcoal; hydrogen / ethanol; ethyl acetate / 1 h / 20 °C / 760.05 Torr / Inert atmosphere

With potassium permanganate; palladium on activated charcoal; hydrogen; In ethanol; water; acetic acid; ethyl acetate;

DOI:10.1016/j.tet.2011.10.100

Reference yield:

(2S,5R,6R)-2-[(2,2-dimethylpropanoyl)oxy]-methylpenicillanat-6-aminium 4-methylbenzenesulfonate (25031-03-2) → C24H43N3O13S2*C7H8O3S (1415712-86-5)

Guidance literature:

Multi-step reaction with 3 steps

1.1: triethylamine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

1.2: 0.83 h / 0 - 20 °C / Inert atmosphere

2.1: potassium permanganate / water; acetic acid / 1 h / -15 - -10 °C / Inert atmosphere

3.1: palladium on activated charcoal; hydrogen / ethanol; ethyl acetate / 1 h / 20 °C / 760.05 Torr / Inert atmosphere

With potassium permanganate; palladium on activated charcoal; hydrogen; triethylamine; In ethanol; dichloromethane; water; acetic acid; ethyl acetate;

DOI:10.1016/j.tet.2011.10.100

Reference yield:

C20H33NO9S (1415713-04-0) → C24H43N3O13S2*C7H8O3S (1415712-86-5)

Guidance literature:

Multi-step reaction with 4 steps

1.1: sodium iodide / acetone / 20 h / 20 °C / Inert atmosphere

1.2: polymer-supported triphenylphosphine / 1.67 h / 0 - 20 °C / Inert atmosphere

1.3: 4.17 h / 0 - 20 °C / Inert atmosphere

2.1: triethylamine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

2.2: 0.83 h / 0 - 20 °C / Inert atmosphere

3.1: potassium permanganate / water; acetic acid / 1 h / -15 - -10 °C / Inert atmosphere

4.1: palladium on activated charcoal; hydrogen / ethanol; ethyl acetate / 1 h / 20 °C / 760.05 Torr / Inert atmosphere

With potassium permanganate; palladium on activated charcoal; hydrogen; triethylamine; sodium iodide; In ethanol; dichloromethane; water; acetic acid; ethyl acetate; acetone;

DOI:10.1016/j.tet.2011.10.100

upstream raw materials:

C₃₂H₄₉N₃O₁₃S₂

(2S,5R,6R)-2-[(2,2-dimethylpropanoyl)oxy]-methylpenicillanat-6-aminium 4-methylbenzenesulfonate

benzyl N-[2-[2-[2-(2-hydroxyethoxy)ethoxy]ethoxy]ethyl]carbamate

C₂₀H₃₃NO₉S