Technology Process of C29H26ClN5O
There total 6 articles about C29H26ClN5O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine hydrochloride;
In
ethanol;
for 18h;
Reflux;
Enzymatic reaction;
DOI:10.1021/jm300831b
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: nickel(II) chloride hexahydrate; sodium tetrahydroborate / ethanol / 12 h / 25 °C
2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / dichloromethane / 1 h / 0 °C
2.2: 12 h / 20 °C
3.1: 3 h / Reflux
4.1: calcium chloride; iron / ethanol; water / 2 h / Reflux
5.1: pyridine hydrochloride / ethanol / 18 h / Reflux; Enzymatic reaction
With
sodium tetrahydroborate; nickel(II) chloride hexahydrate; pyridine hydrochloride; iron; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; calcium chloride;
In
ethanol; dichloromethane; water;
DOI:10.1021/jm300831b
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 2-picoline borane complex; acetic acid / neat (no solvent) / 3 h / 25 °C
2.1: nickel(II) chloride hexahydrate; sodium tetrahydroborate / ethanol / 12 h / 25 °C
3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / dichloromethane / 1 h / 0 °C
3.2: 12 h / 20 °C
4.1: 3 h / Reflux
5.1: calcium chloride; iron / ethanol; water / 2 h / Reflux
6.1: pyridine hydrochloride / ethanol / 18 h / Reflux; Enzymatic reaction
With
sodium tetrahydroborate; 2-picoline borane complex; nickel(II) chloride hexahydrate; pyridine hydrochloride; iron; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; calcium chloride;
In
ethanol; dichloromethane; water;
DOI:10.1021/jm300831b