Technology Process of C21H17Cl2N5O3S
There total 7 articles about C21H17Cl2N5O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: pyridine / 20 °C
2.1: caesium carbonate / dimethyl sulfoxide / 80 °C
3.1: lithium hydroxide / tetrahydrofuran; methanol / 5 h / 20 °C
4.1: N,N-dimethyl-formamide; oxalyl dichloride / tetrahydrofuran / 0.5 h / 20 °C
5.1: ammonium hydroxide
5.2: 2 h / Reflux
6.1: mercury(II) diacetate / 1,4-dioxane / 0.75 h / Reflux
With
pyridine; ammonium hydroxide; oxalyl dichloride; mercury(II) diacetate; caesium carbonate; N,N-dimethyl-formamide; lithium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; methanol; dimethyl sulfoxide;
DOI:10.1016/j.bmcl.2013.04.014
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: N,N-dimethyl-formamide; oxalyl dichloride / tetrahydrofuran / 0.5 h / 20 °C
2.1: ammonium hydroxide
2.2: 2 h / Reflux
3.1: mercury(II) diacetate / 1,4-dioxane / 0.75 h / Reflux
With
ammonium hydroxide; oxalyl dichloride; mercury(II) diacetate; N,N-dimethyl-formamide;
In
tetrahydrofuran; 1,4-dioxane;
DOI:10.1016/j.bmcl.2013.04.014