C₃₃H₃₇NO₃

Base Information

Chemical Name:C₃₃H₃₇NO₃
CAS No.:1422373-44-1
Molecular Formula:C₃₃H₃₇NO₃
Molecular Weight:495.662
Hs Code.:

C<sub>33</sub>H<sub>37</sub>NO<sub>3</sub>

Synonyms:

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Chemical Property of C₃₃H₃₇NO₃

Chemical Property:

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Technology Process of C₃₃H₃₇NO₃

There total 6 articles about C₃₃H₃₇NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1422373-41-8
tert-butyl (R,R,R,E,E)-2-hydroxy-3-[N-benzyl-N-(α-methylbenzyl)amino]-8-phenylocta-4,7-dienoate

: 1422373-44-1
C₃₃H₃₇NO₃

Guidance literature:: tert-butyl (R,R,R,E,E)-2-hydroxy-3-[N-benzyl-N-(α-methylbenzyl)amino]-8-phenylocta-4,7-dienoate; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 0.5h;

With triethylamine; at -78 - 20 ℃; for 0.5h;
DOI:10.1021/jo302731m

Reference yield:

: 1422373-36-1
tert-butyl (E,E)-7-(triisopropylsilyloxy)hepta-2,4-dienoate

: 1422373-44-1
C₃₃H₃₇NO₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C

1.2: 2 h / -78 °C

1.3: 12 h / -78 - 20 °C

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 16 h / 20 °C

3.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 16 h / 0 - 20 °C

4.1: hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide / ethanol / 16 h / 0 - 20 °C

5.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C

6.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C

6.2: 0.5 h / -78 - 20 °C

With n-butyllithium; oxalyl dichloride; hexaammonium heptamolybdate tetrahydrate; tetrabutyl ammonium fluoride; dihydrogen peroxide; potassium hexamethylsilazane; dimethyl sulfoxide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; ethanol; dichloromethane; toluene;
DOI:10.1021/jo302731m

Reference yield:

: tert-butyl (R,R,R,E)-2-hydroxy-3-[N-benzyl-N-(α-methylbenzyl)amino]-7-(triisopropylsilyloxy)hept-4-enoate

: 1422373-44-1
C₃₃H₃₇NO₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 16 h / 20 °C

2.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 16 h / 0 - 20 °C

3.1: hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide / ethanol / 16 h / 0 - 20 °C

4.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C

5.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C

5.2: 0.5 h / -78 - 20 °C

With oxalyl dichloride; hexaammonium heptamolybdate tetrahydrate; tetrabutyl ammonium fluoride; dihydrogen peroxide; potassium hexamethylsilazane; dimethyl sulfoxide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; ethanol; dichloromethane; toluene;
DOI:10.1021/jo302731m