allyl 2-amino-2-deoxy-N-4-methoxybenzylidine-3,4,6-tri-O-allyl-β-D-glucopyanoside

Base Information

Chemical Name:allyl 2-amino-2-deoxy-N-4-methoxybenzylidine-3,4,6-tri-O-allyl-β-D-glucopyanoside
CAS No.:1336880-26-2
Molecular Formula:C₂₆H₃₅NO₆
Molecular Weight:457.567
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of allyl 2-amino-2-deoxy-N-4-methoxybenzylidine-3,4,6-tri-O-allyl-β-D-glucopyanoside

Chemical Property:

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Technology Process of allyl 2-amino-2-deoxy-N-4-methoxybenzylidine-3,4,6-tri-O-allyl-β-D-glucopyanoside

There total 10 articles about allyl 2-amino-2-deoxy-N-4-methoxybenzylidine-3,4,6-tri-O-allyl-β-D-glucopyanoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51471-40-0
6-(hydroxymethyl)-3-[4-methoxybenzylideneamino]tetrahydropyran-2,4,5-triol

: 106-95-6
allyl bromide

: 1336880-26-2
allyl 2-amino-2-deoxy-N-4-methoxybenzylidine-3,4,6-tri-O-allyl-β-D-glucopyanoside

: allyl 2-amino-2-deoxy-N-4-methoxybenzylidine-3,4,6-tri-O-allyl-α-D-glucopyanoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 16h; Overall yield = 64 %; Overall yield = 984 mg; Inert atmosphere; Schlenk technique;
DOI:10.1039/c4ob02056a

Reference yield:

: C₁₇H₂₃NO₆

: 106-95-6
allyl bromide

: 1336880-26-2
allyl 2-amino-2-deoxy-N-4-methoxybenzylidine-3,4,6-tri-O-allyl-β-D-glucopyanoside

Guidance literature:: C₁₇H₂₃NO₆; With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 1h;

allyl bromide; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1080/10426507.2011.553208

Reference yield:

: 14131-63-6
D-glucosamine hydrochloride

: 1336880-26-2
allyl 2-amino-2-deoxy-N-4-methoxybenzylidine-3,4,6-tri-O-allyl-β-D-glucopyanoside

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / 0.08 h / 20 °C / Inert atmosphere; Schlenk technique

2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 16 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

With sodium hydride; sodium hydroxide; In N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c4ob02056a