C₄₁H₄₅NO₅Si₂

Base Information

Chemical Name:C₄₁H₄₅NO₅Si₂
CAS No.:1315334-96-3
Molecular Formula:C₄₁H₄₅NO₅Si₂
Molecular Weight:687.983
Hs Code.:

C<sub>41</sub>H<sub>45</sub>NO<sub>5</sub>Si<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₁H₄₅NO₅Si₂

Chemical Property:

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Technology Process of C₄₁H₄₅NO₅Si₂

There total 7 articles about C₄₁H₄₅NO₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1315334-94-1
C₃₁H₂₇Br₂NO₅

: 1066-54-2
trimethylsilylacetylene

: 1315334-96-3
C₄₁H₄₅NO₅Si₂

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine; In tetrahydrofuran; at 50 ℃; Inert atmosphere;
DOI:10.1016/j.polymer.2011.06.010

Reference yield:

: 22818-40-2
D-4-hydroxyphenylglycine

: 1315334-96-3
C₄₁H₄₅NO₅Si₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: thionyl chloride / methanol / 0 - 20 °C

2.1: sodium hydrogencarbonate / 1,4-dioxane; water / 0 - 20 °C

3.1: sodium periodate; sodium chloride / water; acetic acid / 0.25 h

3.2: 6 h / 0 - 40 °C

4.1: potassium carbonate / acetone / 3 h / Reflux

5.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; triphenylphosphine / tetrahydrofuran / 20 °C / Inert atmosphere

6.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; triphenylphosphine / tetrahydrofuran / 50 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; sodium periodate; copper(l) iodide; thionyl chloride; sodium hydrogencarbonate; potassium carbonate; triethylamine; triphenylphosphine; sodium chloride; In tetrahydrofuran; 1,4-dioxane; methanol; water; acetic acid; acetone;
DOI:10.1016/j.polymer.2011.06.010

Reference yield:

: 872877-06-0
(R)-N-tert-butoxycarbonyl-4'-hydroxy-3',5'-diiodophenylglycine methyl ester

: 1315334-96-3
C₄₁H₄₅NO₅Si₂

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetone / 3 h / Reflux

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; triphenylphosphine / tetrahydrofuran / 20 °C / Inert atmosphere

3: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; triphenylphosphine / tetrahydrofuran / 50 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate; triethylamine; triphenylphosphine; In tetrahydrofuran; acetone;
DOI:10.1016/j.polymer.2011.06.010