trans-bis([3,5-bis(benzyloxy)benzyl](diphenyl)phosphane)bis((E,E/Z)-3,4-bis[(triisopropylsilyl)ethynyl]-6-(trimethylsilyl)hex-3-en-1,5-diynyl)platinum(II)

Base Information

• Chemical Name: trans-bis([3,5-bis(benzyloxy)benzyl](diphenyl)phosphane)bis((E,E/Z)-3,4-bis[(triisopropylsilyl)ethynyl]-6-(trimethylsilyl)hex-3-en-1,5-diynyl)platinum(II)
• CAS No.: 339562-16-2
• Molecular Formula: C₁₂₈H₁₆₀O₄P₂PtSi₆
• Molecular Weight: 2188.22

Synonyms:

Chemical Property of trans-bis([3,5-bis(benzyloxy)benzyl](diphenyl)phosphane)bis((E,E/Z)-3,4-bis[(triisopropylsilyl)ethynyl]-6-(trimethylsilyl)hex-3-en-1,5-diynyl)platinum(II)

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Useful:

Technology Process of trans-bis([3,5-bis(benzyloxy)benzyl](diphenyl)phosphane)bis((E,E/Z)-3,4-bis[(triisopropylsilyl)ethynyl]-6-(trimethylsilyl)hex-3-en-1,5-diynyl)platinum(II)

There total 1 articles about trans-bis([3,5-bis(benzyloxy)benzyl](diphenyl)phosphane)bis((E,E/Z)-3,4-bis[(triisopropylsilyl)ethynyl]-6-(trimethylsilyl)hex-3-en-1,5-diynyl)platinum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

(((CH3)2CH)3SiCC)2CC(CCH)(CCSi(CH3)3) + trans-bis([3,5-bis(benzyloxy)benzyl](diphenyl)phosphane)dichloroplatinum(II)*0.5CH2Cl2 → trans-bis([3,5-bis(benzyloxy)benzyl](diphenyl)phosphane)bis((E,E/Z)-3,4-bis[(triisopropylsilyl)ethynyl]-6-(trimethylsilyl)hex-3-en-1,5-diynyl)platinum(II) (339562-16-2)

Guidance literature:

With CuI; ((CH₃)2CH)2NH; In tetrahydrofuran; (N2 or Ar); mixing of soln. (Me3SiCC)CC(CCSi(C3H7)3)2(CCH) with PtCl2((C6H5CH2O)2C6H3CH2P(C6H5)2)2, CuI and (C3H7)2NH in dry THF in dark in Schlenk app. for 20 h at 20°C; filtration over SiO2, evapn. in vac.; flash chromy., gel-permeation chromy.; as oil;

DOI:10.1002/1522-2675(20010228)84:2<296::AID-HLCA296>3.0.CO;2-X

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