(+/-)-Kreysigin

Base Information

Chemical Name:(+/-)-Kreysigin
CAS No.:31735-22-5
Molecular Formula:C₂₂H₂₇NO₅
Molecular Weight:385.46
Hs Code.:

Synonyms:

Suppliers and Price of (+/-)-Kreysigin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-Kreysigin

Chemical Property:

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Technology Process of (+/-)-Kreysigin

There total 3 articles about (+/-)-Kreysigin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 47764-93-2
1-(3',4',5'-trimethoxyphenethyl)-2-methyl-6-methoxy-7-benzyloxy-1,2,3,4-tetrahydroisoquinoline

: 31735-22-5,23117-57-9
(+/-)-Kreysigin

Guidance literature:: With boron trifluoride diethyl etherate; thallium(III) trifluoroacetate; In dichloromethane; trifluoroacetic acid; 1.) 0 deg C, 8 h, 2.) room temperature, 20 h;
DOI:10.1021/ja00541a021

Reference yield:

: 38726-41-9,38726-70-4
7-hydroxy-6-methoxy-1-(3',4',5'-trimethoxyphenethyl)-N-methyl-1,2,3,4-tetrahydroisoquinoline

: 31735-22-5,23117-57-9
(+/-)-Kreysigin

Guidance literature:: With methanol; iron(III) chloride; Yield given. Multistep reaction; 1.) dichloromethane, 9 h; 2.) overnight;
DOI:10.1016/00404-0399(50)1037I-