C₁₅⁽¹³⁾CH₁₈⁽²⁾H₃NO₄

Base Information

• Chemical Name: C₁₅⁽¹³⁾CH₁₈⁽²⁾H₃NO₄
• CAS No.: 1028386-90-4
• Molecular Formula: C₁₆H₂₁NO₄
• Molecular Weight: 295.312
• Mol file: 1028386-90-4.mol

Synonyms:

Chemical Property of C₁₅⁽¹³⁾CH₁₈⁽²⁾H₃NO₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅⁽¹³⁾CH₁₈⁽²⁾H₃NO₄

There total 1 articles about C₁₅⁽¹³⁾CH₁₈⁽²⁾H₃NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

1,3,5-Trioxan (110-88-3) + C14(13)CH16(2)H3NO3 (1028386-89-1) → C15(13)CH18(2)H3NO4 (1028386-90-4)

Guidance literature:

Multistep reaction.;

DOI:10.1002/jlcr.1223

Reference yield:

C15(13)CH18(2)H3NO4 (1028386-90-4) → C20(13)CH24(2)H3N3O4S (1028386-95-9)

Guidance literature:

Multi-step reaction with 4 steps

1.1: LiOH; H₂O₂ / tetrahydrofuran; H₂O / 20 °C

1.2: Na₂SO₃ / 0 - 5 °C

1.3: 88 percent / LiOH / H₂O / 65 °C

2.1: 92 percent / DIAD; PPh₃ / tetrahydrofuran / 2 h / 20 °C

3.1: 100 percent / thionyl chloride / CH₂Cl₂ / 20 °C

4.1: 90 percent / K₂CO₃ / CH₂Cl₂

With lithium hydroxide; thionyl chloride; di-isopropyl azodicarboxylate; dihydrogen peroxide; potassium carbonate; triphenylphosphine; In tetrahydrofuran; dichloromethane; water; 2.1: Mitsunobu reaction;

DOI:10.1002/jlcr.1223

Reference yield:

C15(13)CH18(2)H3NO4 (1028386-90-4) → SIL-G(864)W7906

Guidance literature:

Multi-step reaction with 5 steps

1.1: LiOH; H₂O₂ / tetrahydrofuran; H₂O / 20 °C

1.2: Na₂SO₃ / 0 - 5 °C

1.3: 88 percent / LiOH / H₂O / 65 °C

2.1: 92 percent / DIAD; PPh₃ / tetrahydrofuran / 2 h / 20 °C

3.1: 100 percent / thionyl chloride / CH₂Cl₂ / 20 °C

4.1: 90 percent / K₂CO₃ / CH₂Cl₂

5.1: NaOH; MeOH; n-Bu₃P / H₂O

With methanol; lithium hydroxide; sodium hydroxide; thionyl chloride; tributylphosphine; di-isopropyl azodicarboxylate; dihydrogen peroxide; potassium carbonate; triphenylphosphine; In tetrahydrofuran; dichloromethane; water; 2.1: Mitsunobu reaction;

DOI:10.1002/jlcr.1223

upstream raw materials:

1,3,5-Trioxan

C₁₄⁽¹³⁾CH₁₆⁽²⁾H₃NO₃

Downstream raw materials:

C₂₀⁽¹³⁾CH₂₄⁽²⁾H₃N₃O₄S