6,6',6''-benzene-1,3,5-triyl-2,2',2''-trinaphthoic acid

Base Information

Chemical Name:6,6',6''-benzene-1,3,5-triyl-2,2',2''-trinaphthoic acid
CAS No.:1383916-83-3
Molecular Formula:C₃₉H₂₄O₆
Molecular Weight:588.616
Hs Code.:

Synonyms:

Suppliers and Price of 6,6',6''-benzene-1,3,5-triyl-2,2',2''-trinaphthoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 6,6',6''-benzene-1,3,5-triyl-2,2',2''-trinaphthoic acid

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 6,6',6''-benzene-1,3,5-triyl-2,2',2''-trinaphthoic acid

There total 2 articles about 6,6',6''-benzene-1,3,5-triyl-2,2',2''-trinaphthoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1383916-85-5
1,3,5-tri(6-methoxycarbonylnaphthalen-2-yl)benzene

: 1383916-83-3
6,6',6''-benzene-1,3,5-triyl-2,2',2''-trinaphthoic acid

Guidance literature:: 1,3,5-tri(6-methoxycarbonylnaphthalen-2-yl)benzene; With sodium hydroxide; In tetrahydrofuran; methanol; water; Reflux;

With hydrogenchloride; In water; Cooling with ice;
DOI:10.1039/c2cc31792c

Reference yield:

: 33626-98-1
methyl 6-bromo-2-naphthoate

: 1383916-83-3
6,6',6''-benzene-1,3,5-triyl-2,2',2''-trinaphthoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / dimethyl sulfoxide / 12 h / 80 °C / Inert atmosphere

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / methanol; water; toluene / Reflux; Inert atmosphere

3.1: sodium hydroxide / tetrahydrofuran; methanol; water / Reflux

3.2: Cooling with ice

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; sodium carbonate; sodium hydroxide; In tetrahydrofuran; methanol; water; dimethyl sulfoxide; toluene; 2.1: Suzuki coupling;
DOI:10.1039/c2cc31792c