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Cyclopentanone, 3-(1-methylethenyl)-2-(phenylthio)-, trans-

Base Information Edit
  • Chemical Name:Cyclopentanone, 3-(1-methylethenyl)-2-(phenylthio)-, trans-
  • CAS No.:139327-05-2
  • Molecular Formula:C14H16OS
  • Molecular Weight:232.346
  • Hs Code.:
  • Mol file:139327-05-2.mol
Cyclopentanone, 3-(1-methylethenyl)-2-(phenylthio)-, trans-

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Chemical Property of Cyclopentanone, 3-(1-methylethenyl)-2-(phenylthio)-, trans- Edit
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Technology Process of Cyclopentanone, 3-(1-methylethenyl)-2-(phenylthio)-, trans-

There total 16 articles about Cyclopentanone, 3-(1-methylethenyl)-2-(phenylthio)-, trans- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 3 steps
1: 76 percent / CH2Cl2 / 0.17 h
2: 66 percent / CH2Cl2 / 0.33 h / 0 - 25 °C
3: toluene / 1 h / 95 °C
In dichloromethane; toluene;
DOI:10.1007/BF00961237
Guidance literature:
Multi-step reaction with 3 steps
1: 76 percent / CH2Cl2 / 0.17 h
2: 66 percent / CH2Cl2 / 0.33 h / 0 - 25 °C
3: toluene / 1 h / 95 °C
In dichloromethane; toluene;
DOI:10.1007/BF00961237
Guidance literature:
Multi-step reaction with 4 steps
1: 1.) LDA / 1.) hexane, THF, -70 deg C, 5 min, 2.) hexane, THF, a) from -70 deg C to 25 deg C, 1 h, b) 25 deg C, 1.5 h
2: 61 percent / AcOH, 30percent aq. H2O2 / 1.) from 5 deg C to 25 deg C, 20 min, 2.) 25 deg C, 4 h
3: 66 percent / CH2Cl2 / 0.33 h / 0 - 25 °C
4: toluene / 1 h / 95 °C
With dihydrogen peroxide; acetic acid; lithium diisopropyl amide; In dichloromethane; toluene;
DOI:10.1007/BF00961237
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