Technology Process of 9-((RS)-2,3-bis(benzylthio)propyl)adenine
There total 4 articles about 9-((RS)-2,3-bis(benzylthio)propyl)adenine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 22 percent / pyridine / 1) 0 degC 2h 2) room temperature 2 days
2: 1) sodium hydride / DMF 1) 60 degC 1h 2) 100 degC 16h
With
sodium hydride;
In
pyridine;
DOI:10.1135/cccc19813134
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydroxide / H2O / 1) 1 h, room temperature 2) 90 min, 100 degC
2: 22 percent / pyridine / 1) 0 degC 2h 2) room temperature 2 days
3: 1) sodium hydride / DMF 1) 60 degC 1h 2) 100 degC 16h
With
sodium hydroxide; sodium hydride;
In
pyridine; water;
DOI:10.1135/cccc19813134
- Guidance literature:
-
Multi-step reaction with 2 steps
1: Na, liq. NH3
2: 1) sodium hydride / DMF 1) 60 degC 1h 2) 100 degC 16h
With
ammonia; sodium; sodium hydride;
DOI:10.1135/cccc19813134
