9-((RS)-2,3-bis(benzylthio)propyl)adenine

Base Information

Chemical Name:9-((RS)-2,3-bis(benzylthio)propyl)adenine
CAS No.:81546-95-4
Molecular Formula:C₂₂H₂₃N₅S₂
Molecular Weight:421.59
Hs Code.:

Synonyms:

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Chemical Property of 9-((RS)-2,3-bis(benzylthio)propyl)adenine

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Technology Process of 9-((RS)-2,3-bis(benzylthio)propyl)adenine

There total 4 articles about 9-((RS)-2,3-bis(benzylthio)propyl)adenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 55487-29-1
2,3-bis(benzylthio)-1-propanol

: 81546-95-4
9-((RS)-2,3-bis(benzylthio)propyl)adenine

Guidance literature:: Multi-step reaction with 2 steps

1: 22 percent / pyridine / 1) 0 degC 2h 2) room temperature 2 days

2: 1) sodium hydride / DMF 1) 60 degC 1h 2) 100 degC 16h

With sodium hydride; In pyridine;
DOI:10.1135/cccc19813134

Reference yield:

: 100-44-7
benzyl chloride

: 81546-95-4
9-((RS)-2,3-bis(benzylthio)propyl)adenine

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / H₂O / 1) 1 h, room temperature 2) 90 min, 100 degC

2: 22 percent / pyridine / 1) 0 degC 2h 2) room temperature 2 days

3: 1) sodium hydride / DMF 1) 60 degC 1h 2) 100 degC 16h

With sodium hydroxide; sodium hydride; In pyridine; water;
DOI:10.1135/cccc19813134

Reference yield:

: 81546-93-2
9-((RS)-2-phenyl-1,3-dithiolane-4-ylmethyl)adenine

: 81546-95-4
9-((RS)-2,3-bis(benzylthio)propyl)adenine

Guidance literature:: Multi-step reaction with 2 steps

1: Na, liq. NH₃

2: 1) sodium hydride / DMF 1) 60 degC 1h 2) 100 degC 16h

With ammonia; sodium; sodium hydride;
DOI:10.1135/cccc19813134