(S)-6-OH-α-Me-Dopa

Base Information

Chemical Name:(S)-6-OH-α-Me-Dopa
CAS No.:72746-40-8
Molecular Formula:C₁₀H₁₃NO₅
Molecular Weight:227.217
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-6-OH-α-Me-Dopa

Chemical Property:

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Technology Process of (S)-6-OH-α-Me-Dopa

There total 6 articles about (S)-6-OH-α-Me-Dopa which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 134040-35-0,17231-84-4
2,4,5-trimethoxy-β-methyl-β-nitrostyrene

: 72746-40-8
(S)-6-OH-α-Me-Dopa

Guidance literature:: Multi-step reaction with 6 steps

1: 75 percent / Fe / acetic acid / 3 h / Heating

2: 81 percent / (NH₄)2CO₃ / ethanol; H₂O / 6.5 h / Heating

3: 67 percent / BaCO₃*8H₂O / H₂O / 48 h / Heating

4: 1.) 1N ethanolic HCl, 3A molecular sieves, 2.) 0.5N aq. NaOH / 12 h / Heating

6: 48percent aq. HBr, glacial acetic acid, 50W-X₈ ion exchange resin (H+ form) / 3 h

With hydrogenchloride; sodium hydroxide; 3 A molecular sieve; 50W-X₈ ion exchange resin (H+ form); hydrogen bromide; ammonium carbonate; iron; acetic acid; barium carbonate; In ethanol; water; acetic acid;
DOI:10.1021/jm00186a007

Reference yield:

: 2020-90-8
2,4,5-Trimethoxyphenylacetone

: 72746-40-8
(S)-6-OH-α-Me-Dopa

Guidance literature:: Multi-step reaction with 5 steps

1: 81 percent / (NH₄)2CO₃ / ethanol; H₂O / 6.5 h / Heating

2: 67 percent / BaCO₃*8H₂O / H₂O / 48 h / Heating

3: 1.) 1N ethanolic HCl, 3A molecular sieves, 2.) 0.5N aq. NaOH / 12 h / Heating

5: 48percent aq. HBr, glacial acetic acid, 50W-X₈ ion exchange resin (H+ form) / 3 h

With hydrogenchloride; sodium hydroxide; 3 A molecular sieve; 50W-X₈ ion exchange resin (H+ form); hydrogen bromide; ammonium carbonate; acetic acid; barium carbonate; In ethanol; water;
DOI:10.1021/jm00186a007

Reference yield:

: 75014-02-7
(RS)-5-methyl-5-(2,4,5-trimethoxyphenyl)hydantoin

: 72746-40-8
(S)-6-OH-α-Me-Dopa

Guidance literature:: Multi-step reaction with 4 steps

1: 67 percent / BaCO₃*8H₂O / H₂O / 48 h / Heating

2: 1.) 1N ethanolic HCl, 3A molecular sieves, 2.) 0.5N aq. NaOH / 12 h / Heating

4: 48percent aq. HBr, glacial acetic acid, 50W-X₈ ion exchange resin (H+ form) / 3 h

With hydrogenchloride; sodium hydroxide; 3 A molecular sieve; 50W-X₈ ion exchange resin (H+ form); hydrogen bromide; acetic acid; barium carbonate; In water;
DOI:10.1021/jm00186a007