C₂₂H₂₆O₆

Base Information

Chemical Name:C₂₂H₂₆O₆
CAS No.:1337894-54-8
Molecular Formula:C₂₂H₂₆O₆
Molecular Weight:386.445
Hs Code.:

C<sub>22</sub>H<sub>26</sub>O<sub>6</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₆O₆

Chemical Property:

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Technology Process of C₂₂H₂₆O₆

There total 5 articles about C₂₂H₂₆O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: C₂₇H₃₄O₇

: C₂₂H₂₆O₆

: 1337894-61-7
C₂₂H₂₆O₆

: 1337894-54-8
C₂₂H₂₆O₆

Guidance literature:: With toluene-4-sulfonic acid; In methanol; at 20 ℃; for 2.4h; optical yield given as %ee;
DOI:10.1039/c1cc13650j

Reference yield:

: 71135-95-0
methyl 2,2-dimethyl-6-oxocyclohexanecarboxylate

: C₂₂H₂₆O₆

: 1337894-54-8
C₂₂H₂₆O₆

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium methanolate / 0 °C / Inert atmosphere

1.2: Reflux; Inert atmosphere

2.1: toluene-4-sulfonic acid / methanol / 0 °C

3.1: oxone / methanol / 20 °C

4.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 2.7 h / 0 °C / Inert atmosphere

5.1: toluene-4-sulfonic acid / methanol / 2.4 h / 20 °C

With dmap; oxone; potassium methanolate; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; In methanol; dichloromethane;
DOI:10.1039/c1cc13650j

Reference yield:

: 1264263-91-3
C₁₅H₂₂O₃

: C₂₂H₂₆O₆

: 1337894-54-8
C₂₂H₂₆O₆

Guidance literature:: Multi-step reaction with 3 steps

1: oxone / methanol / 20 °C

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 2.7 h / 0 °C / Inert atmosphere

3: toluene-4-sulfonic acid / methanol / 2.4 h / 20 °C

With dmap; oxone; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; In methanol; dichloromethane;
DOI:10.1039/c1cc13650j