Succinic acid (3S,8S,9S,10R,13S,14S,17S)-17-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester 2-trimethylsilanyl-ethyl ester

Base Information

Chemical Name:Succinic acid (3S,8S,9S,10R,13S,14S,17S)-17-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester 2-trimethylsilanyl-ethyl ester
CAS No.:114846-95-6
Molecular Formula:C₅₀H₆₆O₇Si
Molecular Weight:807.155
Hs Code.:

Succinic acid (3S,8S,9S,10R,13S,14S,17S)-17-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester 2-trimethylsilanyl-ethyl ester

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Chemical Property of Succinic acid (3S,8S,9S,10R,13S,14S,17S)-17-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester 2-trimethylsilanyl-ethyl ester

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Technology Process of Succinic acid (3S,8S,9S,10R,13S,14S,17S)-17-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester 2-trimethylsilanyl-ethyl ester

There total 3 articles about Succinic acid (3S,8S,9S,10R,13S,14S,17S)-17-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester 2-trimethylsilanyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 114846-95-6
Succinic acid (3S,8S,9S,10R,13S,14S,17S)-17-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester 2-trimethylsilanyl-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / pyridine / 24 h / Ambient temperature

2: 4-dimethylaminopyridine, N,N'-dicyclohexylcarbodiimide / benzene; pyridine / 48 h / Ambient temperature

With dmap; dicyclohexyl-carbodiimide; In pyridine; benzene;

Reference yield:

: 54668-68-7
21-nor-5-pregnene-3β,20-diol

: 114846-95-6
Succinic acid (3S,8S,9S,10R,13S,14S,17S)-17-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester 2-trimethylsilanyl-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / pyridine / 24 h / Ambient temperature

2: 4-dimethylaminopyridine, N,N'-dicyclohexylcarbodiimide / benzene; pyridine / 48 h / Ambient temperature

With dmap; dicyclohexyl-carbodiimide; In pyridine; benzene;