(S)-2-((S)-5-(3-phenylpropyl)-2,4,7,10-tetraoxaundecan-11-yl)-oxirane

Base Information

Chemical Name:(S)-2-((S)-5-(3-phenylpropyl)-2,4,7,10-tetraoxaundecan-11-yl)-oxirane
CAS No.:1261074-46-7
Molecular Formula:C₁₈H₂₈O₅
Molecular Weight:324.417
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-((S)-5-(3-phenylpropyl)-2,4,7,10-tetraoxaundecan-11-yl)-oxirane

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Technology Process of (S)-2-((S)-5-(3-phenylpropyl)-2,4,7,10-tetraoxaundecan-11-yl)-oxirane

There total 4 articles about (S)-2-((S)-5-(3-phenylpropyl)-2,4,7,10-tetraoxaundecan-11-yl)-oxirane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1261074-39-8
(S)-11-phenyl-5-(3-phenylprop-2-ynyl)-2,4,7,10-tetraoxaundecane

: 1261074-46-7
(S)-2-((S)-5-(3-phenylpropyl)-2,4,7,10-tetraoxaundecan-11-yl)-oxirane

Guidance literature:: Multi-step reaction with 2 steps

1.1: palladium 10% on activated carbon; hydrogen; acetic acid / ethanol / 16 h / 20 °C

2.1: N-benzyl-N,N,N-triethylammonium chloride / 0.05 h

2.2: 22.25 h / 20 °C

With palladium 10% on activated carbon; N-benzyl-N,N,N-triethylammonium chloride; hydrogen; acetic acid; In ethanol;
DOI:10.1021/jm101053k

Reference yield:

: 406218-43-7
(S)-2-((2-(benzyloxy)ethoxy)methyl)oxirane

: 1261074-46-7
(S)-2-((S)-5-(3-phenylpropyl)-2,4,7,10-tetraoxaundecan-11-yl)-oxirane

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.75 h / -78 °C / Inert atmosphere

1.2: 0.5 h / Inert atmosphere

1.3: 3 h / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 h / 0 - 20 °C / Inert atmosphere

3.1: palladium 10% on activated carbon; hydrogen; acetic acid / ethanol / 16 h / 20 °C

4.1: N-benzyl-N,N,N-triethylammonium chloride / 0.05 h

4.2: 22.25 h / 20 °C

With n-butyllithium; palladium 10% on activated carbon; N-benzyl-N,N,N-triethylammonium chloride; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; hexane; dichloromethane;
DOI:10.1021/jm101053k

Reference yield:

: C₂₀H₂₂O₃

: 1261074-46-7
(S)-2-((S)-5-(3-phenylpropyl)-2,4,7,10-tetraoxaundecan-11-yl)-oxirane

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 h / 0 - 20 °C / Inert atmosphere

2.1: palladium 10% on activated carbon; hydrogen; acetic acid / ethanol / 16 h / 20 °C

3.1: N-benzyl-N,N,N-triethylammonium chloride / 0.05 h

3.2: 22.25 h / 20 °C

With palladium 10% on activated carbon; N-benzyl-N,N,N-triethylammonium chloride; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane;
DOI:10.1021/jm101053k