C₅(3,5-C₆H₃Me₂)5Br

Base Information

Chemical Name:C₅(3,5-C₆H₃Me₂)5Br
CAS No.:481726-49-2
Molecular Formula:C₄₅H₄₅Br
Molecular Weight:665.756
Hs Code.:

C<sub>5</sub>(3,5-C<sub>6</sub>H<sub>3</sub>Me<sub>2</sub>)5Br

Synonyms:

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Chemical Property of C₅(3,5-C₆H₃Me₂)5Br

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Technology Process of C₅(3,5-C₆H₃Me₂)5Br

There total 6 articles about C₅(3,5-C₆H₃Me₂)5Br which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-67-8
1,3,5-trimethyl-benzene

: 481726-49-2
C₅(3,5-C₆H₃Me₂)5Br

Guidance literature:: Multi-step reaction with 7 steps

1.1: 87 percent / Br₂ / 140 °C

2.1: HCHO; HMTA / H₂O

3.1: KCN / H₂O

4.1: NH₄NO₃

5.1: 75 percent / benzyltrimethylammonium hydroxide / ethanol / 0.25 h / Heating

6.1: toluene; tetrahydrofuran / -80 °C

6.2: 63 percent / aq. NH₄Cl / 20 °C

7.1: 95 percent / SOBr₂; pyridine / CH₂Cl₂ / -10 - 20 °C

With pyridine; ammonium nitrate; potassium cyanide; sulfurous dibromide; formaldehyd; hexamethylenetetramine; bromine; N-benzyl-trimethylammonium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water; toluene; 1.1: Kadesh-Shacklett reaction;
DOI:10.1016/S0022-328X(01)00725-2

Reference yield:

: 5779-95-3
3,5-dimethylbenzaldehyde

: 481726-49-2
C₅(3,5-C₆H₃Me₂)5Br

Guidance literature:: Multi-step reaction with 5 steps

1.1: KCN / H₂O

2.1: NH₄NO₃

3.1: 75 percent / benzyltrimethylammonium hydroxide / ethanol / 0.25 h / Heating

4.1: toluene; tetrahydrofuran / -80 °C

4.2: 63 percent / aq. NH₄Cl / 20 °C

5.1: 95 percent / SOBr₂; pyridine / CH₂Cl₂ / -10 - 20 °C

With pyridine; ammonium nitrate; potassium cyanide; sulfurous dibromide; N-benzyl-trimethylammonium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water; toluene;
DOI:10.1016/S0022-328X(01)00725-2

Reference yield:

: 21918-35-4
1,3-bis(3,5-dimethylphenyl)-2-propanone

: 481726-49-2
C₅(3,5-C₆H₃Me₂)5Br

Guidance literature:: Multi-step reaction with 3 steps

1.1: 75 percent / benzyltrimethylammonium hydroxide / ethanol / 0.25 h / Heating

2.1: toluene; tetrahydrofuran / -80 °C

2.2: 63 percent / aq. NH₄Cl / 20 °C

3.1: 95 percent / SOBr₂; pyridine / CH₂Cl₂ / -10 - 20 °C

With pyridine; sulfurous dibromide; N-benzyl-trimethylammonium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; toluene;
DOI:10.1016/S0022-328X(01)00725-2