(S)-N-((S)-1-amino-3-(4-tert-butoxyphenyl)-1-oxopropan-2-yl)-2-((2Z,5Z)-5-(4-hydroxy-3,5-dimethoxybenzylidene)-4-oxo-2-(phenylimino)thiazolidin-3-yl)propanamide

Base Information

• Chemical Name: (S)-N-((S)-1-amino-3-(4-tert-butoxyphenyl)-1-oxopropan-2-yl)-2-((2Z,5Z)-5-(4-hydroxy-3,5-dimethoxybenzylidene)-4-oxo-2-(phenylimino)thiazolidin-3-yl)propanamide
• CAS No.: 1082954-23-1
• Molecular Formula: C₃₄H₃₈N₄O₇S
• Molecular Weight: 646.764

Synonyms:

Chemical Property of (S)-N-((S)-1-amino-3-(4-tert-butoxyphenyl)-1-oxopropan-2-yl)-2-((2Z,5Z)-5-(4-hydroxy-3,5-dimethoxybenzylidene)-4-oxo-2-(phenylimino)thiazolidin-3-yl)propanamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (S)-N-((S)-1-amino-3-(4-tert-butoxyphenyl)-1-oxopropan-2-yl)-2-((2Z,5Z)-5-(4-hydroxy-3,5-dimethoxybenzylidene)-4-oxo-2-(phenylimino)thiazolidin-3-yl)propanamide

There total 2 articles about (S)-N-((S)-1-amino-3-(4-tert-butoxyphenyl)-1-oxopropan-2-yl)-2-((2Z,5Z)-5-(4-hydroxy-3,5-dimethoxybenzylidene)-4-oxo-2-(phenylimino)thiazolidin-3-yl)propanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-N-((S)-1-amino-3-(4-t-butyoxyphenyl)-1-oxopropan-2-yl)-2-((Z)-4-oxo-2-(phenylimino)thiazolidin-3-yl)propionamide (1082954-15-1) + syringic aldehyde (134-96-3) → (S)-N-((S)-1-amino-3-(4-tert-butoxyphenyl)-1-oxopropan-2-yl)-2-((2Z,5Z)-5-(4-hydroxy-3,5-dimethoxybenzylidene)-4-oxo-2-(phenylimino)thiazolidin-3-yl)propanamide (1082954-23-1)

Guidance literature:

With piperidine; In ethanol; hexane; for 19h; Inert atmosphere; Reflux;

DOI:10.1021/jm8004515

Reference yield:

→ (S)-N-((S)-1-amino-3-(4-tert-butoxyphenyl)-1-oxopropan-2-yl)-2-((2Z,5Z)-5-(4-hydroxy-3,5-dimethoxybenzylidene)-4-oxo-2-(phenylimino)thiazolidin-3-yl)propanamide (1082954-23-1)

Guidance literature:

Reference yield:

(S)-N-((S)-1-amino-3-(4-tert-butoxyphenyl)-1-oxopropan-2-yl)-2-((2Z,5Z)-5-(4-hydroxy-3,5-dimethoxybenzylidene)-4-oxo-2-(phenylimino)thiazolidin-3-yl)propanamide (1082954-23-1) + trifluoroacetic acid (76-05-1) → (S)-N-((S)-1-amino-3-(4-hydroxyphenyl)-1-oxopropan-2-yl)-2-((2Z,5Z)-5-(4-hydroxy-3,5-dimethoxybenzylidene)-4-oxo-2-(phenylimino)thiazolidin-3-yl)propanamide trifluoroacetic acid (1194838-39-5)

Guidance literature:

at 0 ℃; for 0.25h; Inert atmosphere;

DOI:10.1021/jm8004515

upstream raw materials:

(S)-N-((S)-1-amino-3-(4-t-butyoxyphenyl)-1-oxopropan-2-yl)-2-((Z)-4-oxo-2-(phenylimino)thiazolidin-3-yl)propionamide

syringic aldehyde

Downstream raw materials:

(S)-N-((S)-1-amino-3-(4-hydroxyphenyl)-1-oxopropan-2-yl)-2-((2Z,5Z)-5-(4-hydroxy-3,5-dimethoxybenzylidene)-4-oxo-2-(phenylimino)thiazolidin-3-yl)propanamide trifluoroacetic acid

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