1,2-bisethane

Base Information

Chemical Name:1,2-bisethane
CAS No.:23582-00-5
Molecular Formula:C₅₈H₆₀P₆
Molecular Weight:942.957
Hs Code.:

1,2-bis<bis(β-diphenylphosphinoethyl)phosphino>ethane

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Suppliers and Price of 1,2-bisethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-bisethane

Chemical Property:

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Technology Process of 1,2-bisethane

There total 1 articles about 1,2-bisethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23582-00-5
1,2-bisethane

Guidance literature:: Diphenylvinylphosphin, 1,2-Diphosphinoethan, Phenyllithium;
DOI:10.1021/ja00746a011

Reference yield: 43.0%

: 14040-11-0
tungsten hexacarbonyl

: 23582-00-5
1,2-bisethane

: 1,1,4,4-tetrakis(2-diphenylphosphinoethyl)-1,4-diphosphabutane-hexakis(pentacarbonyltungsten)

Guidance literature:: With Me₃NO; In dichloromethane; acetonitrile; stirring W(CO6) with equimolar amt. Me3NO in MeCN/CH2Cl2=1:5 v/v at 0°C (to formation of yellow suspn.), dropwise addn. od stoich. amt. phosphine (in CH2Cl2) over 2 h (stirring), stirring at 0°C for 16 h; evapn. (reduced pressure), recrystn. (MeOH/PhMe); elem. anal.;
DOI:10.1016/S0020-1693(97)05747-2

Reference yield:

: 13985-78-9
tetraethylammonium hexacarbonylvanadium(-1)

: 23582-00-5
1,2-bisethane

: Dicarbonyl(1.2-bis[bis(β-diphenylphosphinoethyl)phosphino]ethane)hydridovanadium(+I)

Guidance literature:: In tetrahydrofuran; Irradiation (UV/VIS); (N2), irradiated for 7 h, volume reduced, chromd. on silica gel with THF, left to stand at room temp. for 1 day, concd., irradiated for 2.5 h; volume reduced, solvent removed with a stream of N2, dried for 10 min under high vacuum, elem. anal.;