(+/-)-1-{4-[(benzyloxy)methyl]cyclopent-3-en-1-yl}uracil

Base Information

Chemical Name:(+/-)-1-{4-[(benzyloxy)methyl]cyclopent-3-en-1-yl}uracil
CAS No.:933993-24-9
Molecular Formula:C₁₇H₁₈N₂O₃
Molecular Weight:298.342
Hs Code.:

Synonyms:

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Chemical Property of (+/-)-1-{4-[(benzyloxy)methyl]cyclopent-3-en-1-yl}uracil

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Technology Process of (+/-)-1-{4-[(benzyloxy)methyl]cyclopent-3-en-1-yl}uracil

There total 5 articles about (+/-)-1-{4-[(benzyloxy)methyl]cyclopent-3-en-1-yl}uracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₄H₂₂N₂O₄

: 933993-24-9
(+/-)-1-{4-[(benzyloxy)methyl]cyclopent-3-en-1-yl}uracil

Guidance literature:: With sodium hydroxide; In methanol; at 20 ℃;
DOI:10.1135/cccc20061011

Reference yield:

: 153186-83-5
(+/-)-3-[(benzyloxy)methyl]cyclopent-3-en-1-ol

: 2775-87-3
3-N-benzoyluracil

: 933993-24-9
(+/-)-1-{4-[(benzyloxy)methyl]cyclopent-3-en-1-yl}uracil

: C₁₇H₁₈O₃N₂

Guidance literature:: (+/-)-3-[(benzyloxy)methyl]cyclopent-3-en-1-ol; 3-N-benzoyluracil; With di-isopropyl azodicarboxylate; triphenylphosphine; In acetonitrile; at -40 ℃; for 2h;

With sodium hydroxide; In methanol; for 12h; Further stages.;
DOI:10.1080/15257770701507937

Reference yield:

: 153186-83-5
(+/-)-3-[(benzyloxy)methyl]cyclopent-3-en-1-ol

: 933993-24-9
(+/-)-1-{4-[(benzyloxy)methyl]cyclopent-3-en-1-yl}uracil

Guidance literature:: Multi-step reaction with 2 steps

1: PPh₃; DIAD / acetonitrile / -40 - 20 °C

2: 486 mg / NaOH / methanol / 20 °C

With sodium hydroxide; di-isopropyl azodicarboxylate; triphenylphosphine; In methanol; acetonitrile;
DOI:10.1135/cccc20061011