(S)-4-[(S)-2-Amino-6-(2,2,2-trichloro-ethoxycarbonylamino)-hexanoylamino]-4-((S)-1,3-dicarbamoyl-propylcarbamoyl)-butyric acid tert-butyl ester; compound with toluene-4-sulfonic acid

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Chemical Name:(S)-4-[(S)-2-Amino-6-(2,2,2-trichloro-ethoxycarbonylamino)-hexanoylamino]-4-((S)-1,3-dicarbamoyl-propylcarbamoyl)-butyric acid tert-butyl ester; compound with toluene-4-sulfonic acid
CAS No.:86096-03-9
Molecular Formula:C₇H₈O₃S*C₂₃H₃₉Cl₃N₆O₈
Molecular Weight:806.162
Hs Code.:

(S)-4-[(S)-2-Amino-6-(2,2,2-trichloro-ethoxycarbonylamino)-hexanoylamino]-4-((S)-1,3-dicarbamoyl-propylcarbamoyl)-butyric acid tert-butyl ester; compound with toluene-4-sulfonic acid

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Chemical Property of (S)-4-[(S)-2-Amino-6-(2,2,2-trichloro-ethoxycarbonylamino)-hexanoylamino]-4-((S)-1,3-dicarbamoyl-propylcarbamoyl)-butyric acid tert-butyl ester; compound with toluene-4-sulfonic acid

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Technology Process of (S)-4-[(S)-2-Amino-6-(2,2,2-trichloro-ethoxycarbonylamino)-hexanoylamino]-4-((S)-1,3-dicarbamoyl-propylcarbamoyl)-butyric acid tert-butyl ester; compound with toluene-4-sulfonic acid

There total 3 articles about (S)-4-[(S)-2-Amino-6-(2,2,2-trichloro-ethoxycarbonylamino)-hexanoylamino]-4-((S)-1,3-dicarbamoyl-propylcarbamoyl)-butyric acid tert-butyl ester; compound with toluene-4-sulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 47594-83-2
α-Benzyloxycarbonyl-ε-troc-L-lysine

: 86096-03-9
(S)-4-[(S)-2-Amino-6-(2,2,2-trichloro-ethoxycarbonylamino)-hexanoylamino]-4-((S)-1,3-dicarbamoyl-propylcarbamoyl)-butyric acid tert-butyl ester; compound with toluene-4-sulfonic acid

Guidance literature:: Multi-step reaction with 3 steps

1: dicyclohexylcarbodiimide / from 0 deg C to r.t.

2: 65 percent / N-methyl-morpholine / Ambient temperature

3: H₂ / 5percent Pd/C / dimethylformamide / 8 h

With 4-methyl-morpholine; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)97641-0

Reference yield:

: (S)-2-Benzyloxycarbonylamino-6-(2,2,2-trichloro-ethoxycarbonylamino)-hexanoic acid 2,5-dioxo-pyrrolidin-1-yl ester

: 86096-03-9
(S)-4-[(S)-2-Amino-6-(2,2,2-trichloro-ethoxycarbonylamino)-hexanoylamino]-4-((S)-1,3-dicarbamoyl-propylcarbamoyl)-butyric acid tert-butyl ester; compound with toluene-4-sulfonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / N-methyl-morpholine / Ambient temperature

2: H₂ / 5percent Pd/C / dimethylformamide / 8 h

With 4-methyl-morpholine; hydrogen; palladium on activated charcoal; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)97641-0