10-oxo-3-methyl-5,5-diphenyl-5-sila-5H,10H,11H-benzopyrido<5,4-b>azepine

Base Information

• Chemical Name: 10-oxo-3-methyl-5,5-diphenyl-5-sila-5H,10H,11H-benzopyrido<5,4-b>azepine
• CAS No.: 89052-48-2
• Molecular Formula: C₂₅H₂₀N₂OSi
• Molecular Weight: 392.532

Synonyms:

Chemical Property of 10-oxo-3-methyl-5,5-diphenyl-5-sila-5H,10H,11H-benzopyrido<5,4-b>azepine

Chemical Property:

Purity/Quality:

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Technology Process of 10-oxo-3-methyl-5,5-diphenyl-5-sila-5H,10H,11H-benzopyrido<5,4-b>azepine

There total 1 articles about 10-oxo-3-methyl-5,5-diphenyl-5-sila-5H,10H,11H-benzopyrido<5,4-b>azepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methyl-9,9-diphenyl-10-oximino-9,10-dihydro-9-sila-3-azaanthracene (73624-45-0) → 11-oxo-3-methyl-5,5-diphenyl-5-sila-5H,10H,11H-benzopyrido<4,5-e>azepine (89052-46-0) + 10-oxo-3-methyl-5,5-diphenyl-5-sila-5H,10H,11H-benzopyrido<5,4-b>azepine (89052-48-2)

Guidance literature:

With phosphorus pentachloride; In diethyl ether; at 20 ℃; for 10h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

DOI:10.1007/BF00842841

upstream raw materials:

2-methyl-9,9-diphenyl-10-oximino-9,10-dihydro-9-sila-3-azaanthracene

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