[Cp₂Zr(Cl)(C(Ph)C(CCPh)P(C₆F₅)2)]

Base Information

Chemical Name:[Cp₂Zr(Cl)(C(Ph)C(CCPh)P(C₆F₅)2)]
CAS No.:958635-65-9
Molecular Formula:C₃₈H₂₀ClF₁₀PZr
Molecular Weight:824.212
Hs Code.:

[Cp<sub>2</sub>Zr(Cl)(C(Ph)C(CCPh)P(C<sub>6</sub>F<sub>5</sub>)2)]

Synonyms:

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Chemical Property of [Cp₂Zr(Cl)(C(Ph)C(CCPh)P(C₆F₅)2)]

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Technology Process of [Cp₂Zr(Cl)(C(Ph)C(CCPh)P(C₆F₅)2)]

There total 1 articles about [Cp₂Zr(Cl)(C(Ph)C(CCPh)P(C₆F₅)2)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 866837-25-4
[Cp₂Zr(Cl)(C(Ph)C(CCPh)PCl₂)]

: 344-04-7
bromopentafluorobenzene

: 958635-65-9
[Cp₂Zr(Cl)(C(Ph)C(CCPh)P(C₆F₅)2)]

Guidance literature:: With n-butyllithium; In hexane; toluene; byproducts: LiCl; (Ar); using Schlenk techniques; dissolving of BrC6F5 in toluene; coolingto -78°C; addn. of n-BuLi/hexane; stirring for 5 min at -78.degr ee.C; addn. of soln. of Cp2ZrCl(C(Ph)C(CCPh)PCl2) in MePh at -78°C; stirring for 1 h at ambient temp.; filtration, evapn. to dryness in oil-pump vac., suspending in pentane; drying in vac., elem. anal.;
DOI:10.1021/om7005968

Reference yield: 57.0%

: 958635-65-9
[Cp₂Zr(Cl)(C(Ph)C(CCPh)P(C₆F₅)2)]

: 917-54-4
methyllithium

: 958635-69-3
[Cp₂Zr(Me)(C(Ph)C(CCPh)P(C₆F₅)2)]

Guidance literature:: In tetrahydrofuran; (Ar); using Schlenk techniques; dissolving of Cp2ZrCl(CPhC(CCPh)P(C6F5)2) in THF; cooling to -78°C; addn. of soln. of MeLi (1.3 equiv.) in THF at -78°C; stirring for 2 h at ambient temp.; removal of solvent in vac., dissolving in toluene; filtration, drying todryness; suspending in pentane; filtration, drying in oil-pump vac., el em. anal.;
DOI:10.1021/om7005968