C₂₄H₂₁F₂N₃O₂S

Base Information

Chemical Name:C₂₄H₂₁F₂N₃O₂S
CAS No.:1392116-48-1
Molecular Formula:C₂₄H₂₁F₂N₃O₂S
Molecular Weight:453.512
Hs Code.:

C<sub>24</sub>H<sub>21</sub>F<sub>2</sub>N<sub>3</sub>O<sub>2</sub>S

Synonyms:

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Chemical Property of C₂₄H₂₁F₂N₃O₂S

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Technology Process of C₂₄H₂₁F₂N₃O₂S

There total 3 articles about C₂₄H₂₁F₂N₃O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1181975-86-9
(3-chloropropyl)-(3,5-difluorophenyl)sulfane

: 1392116-47-0
C₁₅H₁₃N₃O₂

: 1392116-48-1
C₂₄H₂₁F₂N₃O₂S

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In N,N-dimethyl-formamide; at 80 ℃;
DOI:10.1016/j.bmcl.2012.06.038

Reference yield:

: 1392116-45-8
C₉H₈IN₃O

: 1392116-48-1
C₂₄H₂₁F₂N₃O₂S

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / toluene / 16 h / Reflux

2: sodium acetate; palladium diacetate; tris-(o-tolyl)phosphine / N,N-dimethyl-formamide / 0.5 h / 160 °C / Microwave irradiation

3: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide / 80 °C

With sodium acetate; palladium diacetate; tetra-(n-butyl)ammonium iodide; sodium hydride; toluene-4-sulfonic acid; tris-(o-tolyl)phosphine; In N,N-dimethyl-formamide; toluene; 2: Heck reaction;
DOI:10.1016/j.bmcl.2012.06.038

Reference yield:

: 1392116-46-9
C₁₅H₁₄IN₃O₂

: 1392116-48-1
C₂₄H₂₁F₂N₃O₂S

Guidance literature:: Multi-step reaction with 2 steps

1: sodium acetate; palladium diacetate; tris-(o-tolyl)phosphine / N,N-dimethyl-formamide / 0.5 h / 160 °C / Microwave irradiation

2: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide / 80 °C

With sodium acetate; palladium diacetate; tetra-(n-butyl)ammonium iodide; sodium hydride; tris-(o-tolyl)phosphine; In N,N-dimethyl-formamide; 1: Heck reaction;
DOI:10.1016/j.bmcl.2012.06.038