Technology Process of C23H29NO9S2
There total 4 articles about C23H29NO9S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate;
In
dichloromethane; water;
for 2h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) sodium ethoxide, 2.) hydrogen; pyridine / 2.) 2percent palladium-charcoal / 1.) ethanol, room temperature, 4 h, 2.) methanol, 30 atm, 48 h; room temperature, 24 h
2: 84 percent / sodium methoxide / methanol / Ambient temperature
3: 13 percent / sodium hydroxide, tetrabutylammonium hydrogensulphate / H2O; CH2Cl2 / 2 h / Ambient temperature
With
pyridine; sodium hydroxide; hydrogen; sodium methylate; sodium ethanolate; tetra(n-butyl)ammonium hydrogensulfate;
palladium on activated charcoal;
In
methanol; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium metaperiodate, sodium hydrogencarbonate / H2O / 2 h / Ambient temperature; sodium hydrogencarbonate was gradually added to neutralise formic acid produced during the reaction
2: 1.) sodium ethoxide, 2.) hydrogen; pyridine / 2.) 2percent palladium-charcoal / 1.) ethanol, room temperature, 4 h, 2.) methanol, 30 atm, 48 h; room temperature, 24 h
3: 84 percent / sodium methoxide / methanol / Ambient temperature
4: 13 percent / sodium hydroxide, tetrabutylammonium hydrogensulphate / H2O; CH2Cl2 / 2 h / Ambient temperature
With
pyridine; sodium hydroxide; sodium periodate; hydrogen; sodium methylate; sodium ethanolate; tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate;
palladium on activated charcoal;
In
methanol; dichloromethane; water;