(S)-1-[(S)-2-((S)-2-Amino-3-benzyloxycarbonyl-propionylamino)-4-methyl-pentanoyl]-pyrrolidine-2-carboxylic acid; compound with trifluoro-acetic acid

Base Information

Chemical Name:(S)-1-[(S)-2-((S)-2-Amino-3-benzyloxycarbonyl-propionylamino)-4-methyl-pentanoyl]-pyrrolidine-2-carboxylic acid; compound with trifluoro-acetic acid
CAS No.:79113-20-5
Molecular Formula:C₂HF₃O₂*C₂₂H₃₁N₃O₆
Molecular Weight:547.529
Hs Code.:

(S)-1-[(S)-2-((S)-2-Amino-3-benzyloxycarbonyl-propionylamino)-4-methyl-pentanoyl]-pyrrolidine-2-carboxylic acid; compound with trifluoro-acetic acid

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Chemical Property of (S)-1-[(S)-2-((S)-2-Amino-3-benzyloxycarbonyl-propionylamino)-4-methyl-pentanoyl]-pyrrolidine-2-carboxylic acid; compound with trifluoro-acetic acid

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Technology Process of (S)-1-[(S)-2-((S)-2-Amino-3-benzyloxycarbonyl-propionylamino)-4-methyl-pentanoyl]-pyrrolidine-2-carboxylic acid; compound with trifluoro-acetic acid

There total 3 articles about (S)-1-[(S)-2-((S)-2-Amino-3-benzyloxycarbonyl-propionylamino)-4-methyl-pentanoyl]-pyrrolidine-2-carboxylic acid; compound with trifluoro-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7536-58-5,98482-77-0
BOC-L-aspartic acid 4-benzyl ester

: 79113-20-5
(S)-1-[(S)-2-((S)-2-Amino-3-benzyloxycarbonyl-propionylamino)-4-methyl-pentanoyl]-pyrrolidine-2-carboxylic acid; compound with trifluoro-acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: N-methylmorpholine / tetrahydrofuran; acetonitrile / -10 °C

2: N-methylmorpholine / tetrahydrofuran; acetonitrile / 8 h / 4 °C

3: anisole

With 4-methyl-morpholine; methoxybenzene; In tetrahydrofuran; acetonitrile;
DOI:10.1248/cpb.29.1390

Reference yield:

: (S)-3-tert-Butoxycarbonylamino-4-ethoxycarbonyloxy-4-oxo-butyric acid benzyl ester

: 79113-20-5
(S)-1-[(S)-2-((S)-2-Amino-3-benzyloxycarbonyl-propionylamino)-4-methyl-pentanoyl]-pyrrolidine-2-carboxylic acid; compound with trifluoro-acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: N-methylmorpholine / tetrahydrofuran; acetonitrile / 8 h / 4 °C

2: anisole

With 4-methyl-morpholine; methoxybenzene; In tetrahydrofuran; acetonitrile;
DOI:10.1248/cpb.29.1390