9,9-Dimethyl-10-methylen-9,10-dihydrophenanthren

Base Information

Chemical Name:9,9-Dimethyl-10-methylen-9,10-dihydrophenanthren
CAS No.:16004-52-7
Molecular Formula:C₁₇H₁₆
Molecular Weight:220.314
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9,9-Dimethyl-10-methylen-9,10-dihydrophenanthren

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Technology Process of 9,9-Dimethyl-10-methylen-9,10-dihydrophenanthren

There total 2 articles about 9,9-Dimethyl-10-methylen-9,10-dihydrophenanthren which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88284-48-4
2-(trimethylsilyl)phenyl trifluoromethanesulfonate

: 503-60-6
3,3-dimethyl-allyl chloride

: 16004-52-7
9,9-Dimethyl-10-methylen-9,10-dihydrophenanthren

: 17024-04-3
9-Isopropyl-phenanthren

Guidance literature:: 3,3-dimethyl-allyl chloride; With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; cesium fluoride; In acetonitrile; at 20 ℃; for 0.25h;

2-(trimethylsilyl)phenyl trifluoromethanesulfonate; In acetonitrile; at 80 ℃; for 3h;
DOI:10.1021/ja001205a

Reference yield:

: 88284-48-4
2-(trimethylsilyl)phenyl trifluoromethanesulfonate

: 870-63-3
prenyl bromide

: 16004-52-7
9,9-Dimethyl-10-methylen-9,10-dihydrophenanthren

: 17024-04-3
9-Isopropyl-phenanthren

Guidance literature:: With cesium fluoride; In acetonitrile; at 80 ℃; for 10h; Overall yield = 47 %; Inert atmosphere;
DOI:10.1021/acs.inorgchem.7b03271