C₃₀H₃₂Cl₂N₆O₃*ClH

Base Information

Chemical Name:C₃₀H₃₂Cl₂N₆O₃*ClH
CAS No.:1404535-81-4
Molecular Formula:C₃₀H₃₂Cl₂N₆O₃*ClH
Molecular Weight:631.989
Hs Code.:

C<sub>30</sub>H<sub>32</sub>Cl<sub>2</sub>N<sub>6</sub>O<sub>3</sub>*ClH

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₀H₃₂Cl₂N₆O₃*ClH

Chemical Property:

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Technology Process of C₃₀H₃₂Cl₂N₆O₃*ClH

There total 21 articles about C₃₀H₃₂Cl₂N₆O₃*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1404532-74-6
{3-[4-(4-butyryl-5-methyl-pyrazol-1-yl)phenylcarbamoyl]-5,6-dichloro-indol-1-yl}acetic acid methyl ester

: 1404535-81-4
C₃₀H₃₂Cl₂N₆O₃*ClH

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; water / methanol

2: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride / 20 °C / Alkaline conditions

With water; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; sodium hydroxide; In methanol;
DOI:10.1021/jm500588w

Reference yield:

: 1404531-95-8
5,6-dichloro-1H-indole-3-carboxylic acid

: 1404535-81-4
C₃₀H₃₂Cl₂N₆O₃*ClH

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / -10 - 20 °C

1.2: 20 °C

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / 1,2-dichloro-ethane / 20 °C

3.1: sodium hydroxide; water / methanol

4.1: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride / 20 °C / Alkaline conditions

With dmap; water; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jm500588w

Reference yield:

: 121859-57-2
5,6-dichloro-1H-indole

: 1404535-81-4
C₃₀H₃₂Cl₂N₆O₃*ClH

Guidance literature:: Multi-step reaction with 6 steps

1.1: diethyl ether / -5 °C

2.1: potassium hydroxide; water / Reflux

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / -10 - 20 °C

3.2: 20 °C

4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / 1,2-dichloro-ethane / 20 °C

5.1: sodium hydroxide; water / methanol

6.1: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride / 20 °C / Alkaline conditions

With dmap; water; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium hydroxide; sodium hydroxide; In methanol; diethyl ether; 1,2-dichloro-ethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jm500588w