N,N''-bis-1,6-hexanediamine tetrahydrobromide

Base Information

Chemical Name:N,N''-bis-1,6-hexanediamine tetrahydrobromide
CAS No.:80686-06-2
Molecular Formula:4BrH*C₃₂H₅₄N₄O₄S₂
Molecular Weight:946.585
Hs Code.:

N,N''-<dithiobis(3,1-propanediyl)>bis<N'-(3,4-dihydroxyphenyl)methyl>-1,6-hexanediamine tetrahydrobromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N''-bis-1,6-hexanediamine tetrahydrobromide

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Technology Process of N,N''-bis-1,6-hexanediamine tetrahydrobromide

There total 5 articles about N,N''-bis-1,6-hexanediamine tetrahydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124-09-4
1,6-Hexanediamine

: 80686-06-2
N,N''-bis-1,6-hexanediamine tetrahydrobromide

Guidance literature:: Multi-step reaction with 5 steps

2: conc. HCl / various solvent(s)

3: 1.) Na; 3.) FeSO₄*7H₂O, oxygen / 1.) liquid ammonia, -40 deg C; 2.) -40 deg C -> r.t.; 3.) 30 min

4: 2.) NaBH₄

5: 48 percent HBr

With hydrogenchloride; sodium tetrahydroborate; hydrogen bromide; oxygen; sodium; In various solvent(s);

Reference yield:

: 14653-67-9
N-<3-<(phenylmethyl)thio>propyl>-1,6-hexanediamine

: 80686-06-2
N,N''-bis-1,6-hexanediamine tetrahydrobromide

Guidance literature:: Multi-step reaction with 4 steps

1: conc. HCl / various solvent(s)

2: 1.) Na; 3.) FeSO₄*7H₂O, oxygen / 1.) liquid ammonia, -40 deg C; 2.) -40 deg C -> r.t.; 3.) 30 min

3: 2.) NaBH₄

4: 48 percent HBr

With hydrogenchloride; sodium tetrahydroborate; hydrogen bromide; oxygen; sodium; In various solvent(s);