Benzoic acid (7R,7aR)-3-oxo-tetrahydro-pyrrolo[1,2-c]oxazol-7-yl ester

Base Information

Chemical Name:Benzoic acid (7R,7aR)-3-oxo-tetrahydro-pyrrolo[1,2-c]oxazol-7-yl ester
CAS No.:126029-44-5
Molecular Formula:C₁₃H₁₃NO₄
Molecular Weight:247.251
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoic acid (7R,7aR)-3-oxo-tetrahydro-pyrrolo[1,2-c]oxazol-7-yl ester

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Technology Process of Benzoic acid (7R,7aR)-3-oxo-tetrahydro-pyrrolo[1,2-c]oxazol-7-yl ester

There total 10 articles about Benzoic acid (7R,7aR)-3-oxo-tetrahydro-pyrrolo[1,2-c]oxazol-7-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95712-41-7
1-methoxymethyloxypent-2(Z)-ene-5-ol

: 126029-44-5
Benzoic acid (7R,7aR)-3-oxo-tetrahydro-pyrrolo[1,2-c]oxazol-7-yl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 1.) NaH; 2.) concd. HCl / 2.) MeOH

2: 75 percent / Ti(iso-PrO)4, diisopropyl l-tartrate, tert-butyl hydroperoxide, molecular sieves 4A

4: 88 percent / K₂CO₃, methyltrioctylammonium chloride

5: H₂ / PdCl₂

6: pyridine

7: NaH / tetrahydrofuran

With titanium(IV) isopropylate; hydrogenchloride; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate; 4 A molecular sieve; hydrogen; Aliquat 336; sodium hydride; potassium carbonate; palladium dichloride; In tetrahydrofuran; pyridine;

Reference yield:

: 89923-31-9
(E)-5-(benzyloxy)pent-2-en-1-ol

: 126029-44-5
Benzoic acid (7R,7aR)-3-oxo-tetrahydro-pyrrolo[1,2-c]oxazol-7-yl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 80 percent / Ti(iso-PrO)4, diisopropyl l-tartrate, tert-butyl hydroperoxide, molecular sieves 4A

3: 88 percent / K₂CO₃, methyltrioctylammonium chloride

4: H₂ / PdCl₂

5: pyridine

6: NaH / tetrahydrofuran

With titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate; 4 A molecular sieve; hydrogen; Aliquat 336; sodium hydride; potassium carbonate; palladium dichloride; In tetrahydrofuran; pyridine;

Reference yield:

: 108275-12-3
1-methoxymethyloxy-2-pentyn-5-ol

: 126029-44-5
Benzoic acid (7R,7aR)-3-oxo-tetrahydro-pyrrolo[1,2-c]oxazol-7-yl ester

Guidance literature:: Multi-step reaction with 8 steps

1: 67 percent / lithium aluminum hydride / tetrahydrofuran; diethyl ether

2: 1.) NaH; 2.) concd. HCl / 2.) MeOH

3: 80 percent / Ti(iso-PrO)4, diisopropyl l-tartrate, tert-butyl hydroperoxide, molecular sieves 4A

5: 88 percent / K₂CO₃, methyltrioctylammonium chloride

6: H₂ / PdCl₂

7: pyridine

8: NaH / tetrahydrofuran

With titanium(IV) isopropylate; hydrogenchloride; tert.-butylhydroperoxide; lithium aluminium tetrahydride; L-(+)-diisopropyl tartrate; 4 A molecular sieve; hydrogen; Aliquat 336; sodium hydride; potassium carbonate; palladium dichloride; In tetrahydrofuran; pyridine; diethyl ether;