Technology Process of fujenal diacid
There total 11 articles about fujenal diacid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 0.5N NaOH / ethanol / 20 h / Heating
2: 20 h / incubations with resuspended mycelium of Gibberella fujikuroi, mutant B1-41a in 0percent N ICI medium at pH=3.5
With
sodium hydroxide;
In
ethanol;
DOI:10.1016/0031-9422(82)80126-X
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 55 mg / 0.5M Na naphthalenide in glyme / tetrahydrofuran / 0.5 h / -63 °C
2: 2 h / incubation with Gibberella fujikuroi, mutant B1-41a
3: 0.5N NaOH / ethanol / 20 h / Heating
4: 20 h / incubations with resuspended mycelium of Gibberella fujikuroi, mutant B1-41a in 0percent N ICI medium at pH=3.5
With
sodium hydroxide; Na naphthalenide in glyme;
In
tetrahydrofuran; ethanol;
DOI:10.1016/0031-9422(82)80126-X
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 293 mg / pyridine / 168 h
2: 112 mg / collidine / various solvent(s) / 13 h / Heating
3: 2 h / incubation with Gibberella fujikuroi, mutant B1-41a
4: 0.5N NaOH / ethanol / 20 h / Heating
5: 20 h / incubations with resuspended mycelium of Gibberella fujikuroi, mutant B1-41a in 0percent N ICI medium at pH=3.5
With
pyridine; 2,3,5-trimethyl-pyridine; sodium hydroxide;
In
ethanol;
DOI:10.1016/0031-9422(82)80126-X