(Z)-7-Decene-1-ol

Base Information

• Chemical Name: (Z)-7-Decene-1-ol
• CAS No.: 52957-12-7
• Molecular Formula: C₁₀H₂₀O
• Molecular Weight: 156.268
• Hs Code.: 2905290000
• NSC Number: 108036,108035
• DSSTox Substance ID: DTXSID50418994
• Nikkaji Number: J2.443.325K
• Wikidata: Q82229759
• Mol file: 52957-12-7.mol

Synonyms:NSC108036;16504-66-8;NSC 108035;(z)-7-decenol;(Z)-7-Decene-1-ol;SCHEMBL8077259;DTXSID50418994;NSC108035;NSC-108035;NSC-108036

Chemical Property of (Z)-7-Decene-1-ol

Chemical Property:

• Vapor Pressure: 0.0111mmHg at 25°C
• Boiling Point: 232.4°Cat760mmHg
• Flash Point: 87.9°C
• PSA: 20.23000
• Density: 0.845g/cm³
• LogP: 2.89540
• XLogP3: 3.1
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 7
• Exact Mass: 156.151415257
• Heavy Atom Count: 11
• Complexity: 86.9

Purity/Quality:

95% ^*data from raw suppliers

(7E)-DEC-7-EN-1-OL 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCC=CCCCCCCO
• Isomeric SMILES: CC/C=C\CCCCCCO

Technology Process of (Z)-7-Decene-1-ol

There total 18 articles about (Z)-7-Decene-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

(E)-1-(2-tetrahydropyranyloxy)-7-decene (73881-17-1) → (E)-7-Decen-1-ol (52957-12-7,16504-66-8)

Guidance literature:

With pyridinium p-toluenesulfonate; In methanol; at 20 ℃; for 24h;

DOI:10.1002/jccs.199900011

Reference yield: 78.0%

7-decyn-1-ol (69222-08-8) → (E)-7-Decen-1-ol (52957-12-7,16504-66-8)

Guidance literature:

With ammonia; sodium; for 2h;

DOI:10.1080/00397919508011480

Reference yield:

1-(2-Tetrahydropyranyloxy)-7-octyne (16695-31-1) → (E)-7-Decen-1-ol (52957-12-7,16504-66-8)

Guidance literature:

Multi-step reaction with 3 steps

1.1: zirconocene chloride hydride / benzene / 6 h / 20 °C

1.2: 71 percent / I₂ / benzene

2.1: Pd(PPh₃)4 / benzene / 0.25 h / 20 °C

2.2: 70 percent / benzene / 20 °C

3.1: 80 percent / PPTs / methanol / 24 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; zirconocene chloride hydride; pyridinium p-toluenesulfonate; In methanol; benzene; 1.1: hydrozirconation / 1.2: Iodination / 2.1: Metallation / 2.2: Condensation / 3.1: deprotection;

DOI:10.1002/jccs.199900011

upstream raw materials:

(E)-dec-7-enoic acid

(E)-1-(2-tetrahydropyranyloxy)-7-decene

7-decyn-1-ol

1-(2-Tetrahydropyranyloxy)-7-octyne

Downstream raw materials:

(E)-7-decenyl acetate