Technology Process of C19H24N2O5S2Se
There total 4 articles about C19H24N2O5S2Se which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: NaBH4 / ethanol
1.2: 94 percent / ethanol / 1 h
2.1: lithium hexamethyldisilylazide / tetrahydrofuran / 0.17 h / -78 °C
2.2: 92 percent / tetrahydrofuran / -78 - 20 °C
3.1: lithium hexamethyldisilylazide / tetrahydrofuran / 0.17 h / -78 °C
3.2: 80 percent / tetrahydrofuran / 14 h / -78 - 20 °C
4.1: 96 percent / trifluoroacetic acid / CH2Cl2 / 2 h / 0 °C
5.1: 70 percent / DCC / CH2Cl2 / 3 h / 20 °C
With
sodium tetrahydroborate; dicyclohexyl-carbodiimide; trifluoroacetic acid; lithium hexamethyldisilazane;
In
tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1039/b409242b
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium hexamethyldisilylazide / tetrahydrofuran / 0.17 h / -78 °C
1.2: 92 percent / tetrahydrofuran / -78 - 20 °C
2.1: lithium hexamethyldisilylazide / tetrahydrofuran / 0.17 h / -78 °C
2.2: 80 percent / tetrahydrofuran / 14 h / -78 - 20 °C
3.1: 96 percent / trifluoroacetic acid / CH2Cl2 / 2 h / 0 °C
4.1: 70 percent / DCC / CH2Cl2 / 3 h / 20 °C
With
dicyclohexyl-carbodiimide; trifluoroacetic acid; lithium hexamethyldisilazane;
In
tetrahydrofuran; dichloromethane;
DOI:10.1039/b409242b
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium hexamethyldisilylazide / tetrahydrofuran / 0.17 h / -78 °C
1.2: 80 percent / tetrahydrofuran / 14 h / -78 - 20 °C
2.1: 96 percent / trifluoroacetic acid / CH2Cl2 / 2 h / 0 °C
3.1: 70 percent / DCC / CH2Cl2 / 3 h / 20 °C
With
dicyclohexyl-carbodiimide; trifluoroacetic acid; lithium hexamethyldisilazane;
In
tetrahydrofuran; dichloromethane;
DOI:10.1039/b409242b