bis(tri-p-tolylphosphine)heptahydridorhenium(VII)

Base Information

• Chemical Name: bis(tri-p-tolylphosphine)heptahydridorhenium(VII)
• CAS No.: 56226-01-8
• Molecular Formula: C₄₂H₄₉P₂Re
• Molecular Weight: 802.006

Synonyms:

Chemical Property of bis(tri-p-tolylphosphine)heptahydridorhenium(VII)

Chemical Property:

Purity/Quality:

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Technology Process of bis(tri-p-tolylphosphine)heptahydridorhenium(VII)

There total 1 articles about bis(tri-p-tolylphosphine)heptahydridorhenium(VII) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ReOCl3(P(p-tolyl)3)2 (108009-08-1,108741-33-9) → bis(tri-p-tolylphosphine)heptahydridorhenium(VII) (56226-01-8)

Guidance literature:

With LiAlH₄; In not given; treated with excess LiAlH4;

DOI:10.1039/c39910000241

Reference yield: 45.0%

bis(tri-p-tolylphosphine)heptahydridorhenium(VII) (56226-01-8) + Cyclopentane (287-92-3) → (C5H5)Re(P(CH3C6H4)3)2H2

Guidance literature:

In not given; biphosphine rhenium heptahydride refluxed with cyclopentane for 1 h;

DOI:10.1039/c39820000606

Reference yield:

bis(tri-p-tolylphosphine)heptahydridorhenium(VII) (56226-01-8) + cyclopenta-1,3-diene (542-92-7,25568-84-7,7313-32-8) → CpRe(P(p-C6H4Me)3)2H2

Guidance literature:

In tetrahydrofuran; THF soln. of the Re-complex was treated with 100 equiv of cyclopentadiene under inert atmosphere followed by gentle heating;

upstream raw materials:

ReOCl₃(P(p-tolyl)3)2

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