7b-benzyl-5-nitro-7bH-cyclopentindene

Base Information

Chemical Name:7b-benzyl-5-nitro-7bH-cyclopentindene
CAS No.:97568-00-8
Molecular Formula:C₁₈H₁₃NO₂
Molecular Weight:275.307
Hs Code.:

7b-benzyl-5-nitro-7bH-cyclopent<cd>indene

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7b-benzyl-5-nitro-7bH-cyclopentindene

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Technology Process of 7b-benzyl-5-nitro-7bH-cyclopentindene

There total 3 articles about 7b-benzyl-5-nitro-7bH-cyclopentindene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7b-Benzyl-2a-methoxy-6,7b-dihydro-2aH-cyclopenta[cd]indene

: 97568-00-8
7b-benzyl-5-nitro-7bH-cyclopentindene

Guidance literature:: Multi-step reaction with 2 steps

1: PTSA / 0.5 h / Ambient temperature

2: copper(II) nitrate trihydrate / acetic anhydride / 2 h / 0 °C

With copper(II) nitrate; toluene-4-sulfonic acid; In acetic anhydride;

Reference yield:

: 97567-97-0,97591-72-5
(2aS,7bS)-7b-Benzyl-2a-methoxy-2a,6,7,7b-tetrahydro-2H-cyclopenta[cd]inden-2-ol

: 97568-00-8
7b-benzyl-5-nitro-7bH-cyclopentindene

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) MTPI; 2.) 10percent sodium hydroxide / 1.) HMPA, room temp., 8 h.; 2.) 1 h.

2: PTSA / 0.5 h / Ambient temperature

3: copper(II) nitrate trihydrate / acetic anhydride / 2 h / 0 °C

With sodium hydroxide; copper(II) nitrate; toluene-4-sulfonic acid; In acetic anhydride;