10-methylenecyclooctadecanone

Base Information

Chemical Name:10-methylenecyclooctadecanone
CAS No.:99605-57-9
Molecular Formula:C₁₉H₃₄O
Molecular Weight:278.478
Hs Code.:

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Suppliers and Price of 10-methylenecyclooctadecanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 10-methylenecyclooctadecanone

Chemical Property:

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Technology Process of 10-methylenecyclooctadecanone

There total 2 articles about 10-methylenecyclooctadecanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 13747-10-9
cyclooctadecane-1,10-dione

: 19493-09-5
Methylenetriphenylphosphorane

: 99605-57-9
10-methylenecyclooctadecanone

Guidance literature:: In tetrahydrofuran; for 20h; Heating;
DOI:10.1021/ja00262a052

Reference yield:

: 75-47-8
iodoform

: 13747-10-9
cyclooctadecane-1,10-dione

: 138152-02-0
1,10-dimethylenecyclooctadecane

: 99605-57-9
10-methylenecyclooctadecanone

Guidance literature:: With titanium tetrachloride; lead(II) chloride; zinc; Yield given. Multistep reaction. Yields of byproduct given; 1) THF, CH₂Cl₂, ice-bath, 15 min; 2) THF, CH₂Cl₂, rt, 24 h;
DOI:10.1021/jo930376d