cis-[Pt(II)(pentafluorophenyl)2(1,3-bis(diphenylphosphino)propane)]

Base Information

Chemical Name:cis-[Pt(II)(pentafluorophenyl)2(1,3-bis(diphenylphosphino)propane)]
CAS No.:875766-02-2
Molecular Formula:C₃₉H₂₆F₁₀P₂Pt
Molecular Weight:941.647
Hs Code.:

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Chemical Property of cis-[Pt(II)(pentafluorophenyl)2(1,3-bis(diphenylphosphino)propane)]

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Technology Process of cis-[Pt(II)(pentafluorophenyl)2(1,3-bis(diphenylphosphino)propane)]

There total 2 articles about cis-[Pt(II)(pentafluorophenyl)2(1,3-bis(diphenylphosphino)propane)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 68558-86-1
thallium(I) pentafluorobenzoate

: 868157-81-7
[dichloroplatinum(II)( μ-1,3-bis(diphenylphosphano)propane)]*CH2Cl2

: 875766-02-2
cis-[Pt(II)(pentafluorophenyl)2(1,3-bis(diphenylphosphino)propane)]

Guidance literature:: In pyridine; byproducts: TlCl, CO2; all manipulations under dry N2 atm.; Pt and Tl compds. (in molar ratio of 1:3-3.5) refluxed with pyridine for various times; solvent removed in vac. at room temp., residue washed with hexane, extd.with acetone, filtered, evapd. to dryness,; elem. anal.;
DOI:10.1002/zaac.200400465

Reference yield: 71.0%

: 68558-86-1
thallium(I) pentafluorobenzoate

: 868157-81-7
[dichloroplatinum(II)( μ-1,3-bis(diphenylphosphano)propane)]*CH2Cl2

: 875766-02-2
cis-[Pt(II)(pentafluorophenyl)2(1,3-bis(diphenylphosphino)propane)]

: 875766-00-0
[Pt(1,2-bis(diphenylphosphano)propane)Cl(C₆F₅)]

Guidance literature:: In pyridine; byproducts: TlCl, CO2; all manipulations under dry N2 atm.; Pt and Tl compds. (in molar ratio of 1:2) refluxed with pyridine for 15 min; solvent removed in vac. at room temp., residue washed with hexane, extd.with acetone, filtered, evapd. to dryness, TLC chromy. (Kieselgel, CHCl 3/CCl4) or column chromy. (Al2O3, acetone/hexane (1:3.5)); elem. anal.;
DOI:10.1002/zaac.200400465