Acetic acid, 2,2'-[1,2-ethanediylbis(oxy)]bis-, bis(pentafluorophenyl) ester

Base Information

Chemical Name:Acetic acid, 2,2'-[1,2-ethanediylbis(oxy)]bis-, bis(pentafluorophenyl) ester
CAS No.:139360-39-7
Molecular Formula:C18H8F10O6
Molecular Weight:510.23700
Hs Code.:
Mol file:139360-39-7.mol

Synonyms:(2-Pentafluorophenyloxycarbonylmethoxy-ethoxy)-acetic acid pentafluorophenyl ester;

Suppliers and Price of Acetic acid, 2,2'-[1,2-ethanediylbis(oxy)]bis-, bis(pentafluorophenyl) ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
Di(Pentafluorophenyl)(ethy1enedioxy)diacetate
250mg
$ 580.00

TRC
Di(Pentafluorophenyl)(ethy1enedioxy)diacetate
50mg
$ 210.00

Crysdot
Di(Pentafluorophenyl)(ethy1enedioxy)diacetate 95+%
1g
$ 790.00

BroadPharm
3,6-dioxoctanedioicacidbis-pfpester 96%
1 G
$ 450.00

Total 1 raw suppliers

Chemical Property of Acetic acid, 2,2'-[1,2-ethanediylbis(oxy)]bis-, bis(pentafluorophenyl) ester

Chemical Property:

PSA：71.06000
LogP:3.62180

Purity/Quality:

>98.00% ^*data from raw suppliers

Di(Pentafluorophenyl)(ethy1enedioxy)diacetate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Acetic acid, 2,2'-[1,2-ethanediylbis(oxy)]bis-, bis(pentafluorophenyl) ester

There total 2 articles about Acetic acid, 2,2'-[1,2-ethanediylbis(oxy)]bis-, bis(pentafluorophenyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 23243-68-7,39927-08-7
3,6-dioxasuberic acid

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 139360-39-7
(ethylenedioxy)diacetic acid pentafluorophenyl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In 1,4-dioxane;
DOI:10.1016/0040-4039(91)80575-Q

Reference yield:

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 112-27-6
2,2'-[1,2-ethanediylbis(oxy)]bisethanol

: 139360-39-7
(ethylenedioxy)diacetic acid pentafluorophenyl ester

: 158573-58-1
oxydiacetic acid pentafluorophenyl ester

Guidance literature:: With nitric acid; dicyclohexyl-carbodiimide; Multistep reaction; 1.) 45 deg C, 2.) 0 deg C, 30 min; r.t., 3.5 h;
DOI:10.1021/jo00088a022

Reference yield:

: 139360-39-7
(ethylenedioxy)diacetic acid pentafluorophenyl ester

: (1R,12S)-24-(4-Chloro-benzyloxy)-5,8,14,17,20,23,25-heptaoxa-2,11-diaza-24-phospha-bicyclo[10.9.5]hexacosane-3,10,13,21-tetraone

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) TFA, 2.) 4-methylmorpholine / 1.) CH₂Cl₂, 0 deg C, 1 h, 2.) THF, r.t., 4 h

2: H₂ / 10percent Pd/C / methanol

3: N,N-diisopropylethylamine / CH₂Cl₂ / Ambient temperature

With 4-methyl-morpholine; hydrogen; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1021/jo00088a022