NH₂OCC₆H₄CH₂NH(CH₂)4NH₂(B₈H₁₁)NH(CH₂)4NHCH₂C₆H₄CONH₂

Base Information

• Chemical Name: NH₂OCC₆H₄CH₂NH(CH₂)4NH₂(B₈H₁₁)NH(CH₂)4NHCH₂C₆H₄CONH₂
• CAS No.: 860293-69-2
• Molecular Formula: C₂₄H₄₈B₈N₆O₂
• Molecular Weight: 539.172
• Mol file: 860293-69-2.mol

Synonyms:

Chemical Property of NH₂OCC₆H₄CH₂NH(CH₂)4NH₂(B₈H₁₁)NH(CH₂)4NHCH₂C₆H₄CONH₂

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of NH₂OCC₆H₄CH₂NH(CH₂)4NH₂(B₈H₁₁)NH(CH₂)4NHCH₂C₆H₄CONH₂

There total 1 articles about NH₂OCC₆H₄CH₂NH(CH₂)4NH₂(B₈H₁₁)NH(CH₂)4NHCH₂C₆H₄CONH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

H3BNH2(CH2)4NH2 (860026-68-2) + (4-aminobutylamine)-(N-aminobutyl)azanonaborane(11) (484050-03-5) + 4-formylbenzamide (6051-41-8) → NH2OCC6H4CH2NH(CH2)4NH2(B8H11)NH(CH2)4NHCH2C6H4CONH2 (860293-69-2)

Guidance literature:

In tetrahydrofuran; carbonyl compd. was added dropwise to soln. of azanonaborane and H3BNH2(CH2)4NH2 in THF at room temp.; mixt. was stirred for 2 d; filtered; volatiles removed (vac.); chromd. (silica gel, THF/CH2Cl2, 1/2); elem. anal.;

DOI:10.1039/b503445k

upstream raw materials:

H₃BNH₂(CH₂)4NH₂

(4-aminobutylamine)-(N-aminobutyl)azanonaborane⁽¹¹⁾

4-formylbenzamide