(P(C₆H₅)3)2N⁽¹⁺⁾*[CH₃C(CH₂P(C₆H₅)2)3Fe(NCCr(CO)5)3]^(1-)=(P(C₆H₅)3)2N[CH₃C(CH₂P(C₆H₅)2)3Fe(NCCr(CO)5)3]

Base Information

• Chemical Name: (P(C₆H₅)3)2N⁽¹⁺⁾*[CH₃C(CH₂P(C₆H₅)2)3Fe(NCCr(CO)5)3]^(1-)=(P(C₆H₅)3)2N[CH₃C(CH₂P(C₆H₅)2)3Fe(NCCr(CO)5)3]
• CAS No.: 459143-70-5
• Molecular Formula: C₃₆H₃₀NP₂*C₅₉H₃₉Cr₃FeN₃O₁₅P₃
• Molecular Weight: 1873.31
• Mol file: 459143-70-5.mol

Synonyms:

Chemical Property of (P(C₆H₅)3)2N⁽¹⁺⁾*[CH₃C(CH₂P(C₆H₅)2)3Fe(NCCr(CO)5)3]^(1-)=(P(C₆H₅)3)2N[CH₃C(CH₂P(C₆H₅)2)3Fe(NCCr(CO)5)3]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (P(C₆H₅)3)2N⁽¹⁺⁾*[CH₃C(CH₂P(C₆H₅)2)3Fe(NCCr(CO)5)3]^(1-)=(P(C₆H₅)3)2N[CH₃C(CH₂P(C₆H₅)2)3Fe(NCCr(CO)5)3]

There total 1 articles about (P(C₆H₅)3)2N⁽¹⁺⁾*[CH₃C(CH₂P(C₆H₅)2)3Fe(NCCr(CO)5)3]^(1-)=(P(C₆H₅)3)2N[CH₃C(CH₂P(C₆H₅)2)3Fe(NCCr(CO)5)3] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

sodium pentacarbonylcyanochromate + bis(triphenylphosphine)iminium chloride (21050-13-5) + iron(II) chloride + [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine] (22031-12-5) → (P(C6H5)3)2N(1+)*[CH3C(CH2P(C6H5)2)3Fe(NCCr(CO)5)3](1-)=(P(C6H5)3)2N[CH3C(CH2P(C6H5)2)3Fe(NCCr(CO)5)3] (459143-70-5)

Guidance literature:

In acetone; Irradiation (UV/VIS); all manipulations under Ar; to soln. of FeCl2 and tripod added soln. of Cr compd. dropwise, then added P compd.; concd. to dryness, residue dissolved in CH2Cl2, stirred for 2 h, filtered, soln. concd., layered with EtOH, elem. anal.;

DOI:10.1002/1099-0682(200111)2001:11<2783::AID-EJIC2783>3.0.CO;2-R

upstream raw materials:

bis(triphenylphosphine)iminium chloride

[2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine]