CH₂CHC₆H₄BBrC₄H₂S₂C₄H₂C₆H₁₃

Base Information

Chemical Name:CH₂CHC₆H₄BBrC₄H₂S₂C₄H₂C₆H₁₃
CAS No.:1082577-52-3
Molecular Formula:C₂₂H₂₄BBrS₂
Molecular Weight:443.28
Hs Code.:

CH<sub>2</sub>CHC<sub>6</sub>H<sub>4</sub>BBrC<sub>4</sub>H<sub>2</sub>S<sub>2</sub>C<sub>4</sub>H<sub>2</sub>C<sub>6</sub>H<sub>13</sub>

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Chemical Property of CH₂CHC₆H₄BBrC₄H₂S₂C₄H₂C₆H₁₃

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Technology Process of CH₂CHC₆H₄BBrC₄H₂S₂C₄H₂C₆H₁₃

There total 1 articles about CH₂CHC₆H₄BBrC₄H₂S₂C₄H₂C₆H₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (5′-hexyl-[2,2′-bithiophen]-5-yl)trimethylstannane

: 1009-43-4
4-(trimethylsilyl)styrene

: 10294-33-4
boron tribromide

: 1082577-52-3
CH₂CHC₆H₄BBrC₄H₂S₂C₄H₂C₆H₁₃

Guidance literature:: In dichloromethane; a soln. of BBr3 in CH2Cl2 was added dropwise to polystyrene-compound in CH2Cl2, stirred for 16 h, a soln. of bithiophene-compound in CH2Cl2 was added dropwise at room temp., the mixt. was stirred for 12 h at room temp.; volatiles were removed under high vac.;
DOI:10.1021/ja063302v

Reference yield:

: 1082577-52-3
CH₂CHC₆H₄BBrC₄H₂S₂C₄H₂C₆H₁₃

: (Cu(mesitylene))*(Toluene)_0.2

: 1082577-56-7
CH₂CHC₆H₄B(C₆H₂(CH₃)3)C₄H₂S₂C₄H₂C₆H₁₃

Guidance literature:: In toluene; Cu-compound in toluene was added dropwise to a soln. of B-compound in toluene, the mixt. was allowed to react for 3 h then refluxed for 72 h; filtered through celite, concd., pptd. into cold hexane, repeated pptn. from toluene into hexane, dried at 50°C under high vac.; elem. anal.;
DOI:10.1021/ja063302v

Reference yield:

: 1082577-52-3
CH₂CHC₆H₄BBrC₄H₂S₂C₄H₂C₆H₁₃

: (Cu(mesitylene))*(Toluene)_0.2

: 133144-35-1
[2,2′-bithiophen]-5-yltrimethylstannane

: CH₂CHC₆H₄B(C₆H₂(CH₃)3)C₄H₂S₂C₄H₃

Guidance literature:: In dichloromethane; BBr3 in CH2Cl2 was added dropwise to polystyrene in CH2Cl2, stirred at room temp., Sn-compound in CH2Cl2 was added, stirred, evapd., Cu-compoundin toluene was added dropwise to B-compound in toluene, 130°C; filtered through celite, concd., pptd. into cold hexane, repeated pptn. from toluene into hexane, dried;
DOI:10.1021/ja063302v