Technology Process of C32H38N2O11
There total 3 articles about C32H38N2O11 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: boron trifluoride diethyl etherate / dichloromethane / 21.8 h / 0 - 20 °C / Inert atmosphere; Darkness
2: tetrabutylammomium bromide / water; chloroform; N,N-dimethyl-formamide / 12 h / 40 °C
3: sodium methylate; methanol / 3 h / 20 °C
With
methanol; boron trifluoride diethyl etherate; tetrabutylammomium bromide; sodium methylate;
In
dichloromethane; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1080/07328303.2012.689041
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogenchloride / ethanol; water; toluene / 36 h / Reflux; Dean-Stark
2: tetrabutylammomium bromide / water; chloroform; N,N-dimethyl-formamide / 12 h / 40 °C
3: sodium methylate; methanol / 3 h / 20 °C
With
hydrogenchloride; methanol; tetrabutylammomium bromide; sodium methylate;
In
ethanol; chloroform; water; N,N-dimethyl-formamide; toluene;
DOI:10.1080/07328303.2012.689041
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrabutylammomium bromide / water; chloroform; N,N-dimethyl-formamide / 12 h / 40 °C
2: sodium methylate; methanol / 3 h / 20 °C
With
methanol; tetrabutylammomium bromide; sodium methylate;
In
chloroform; water; N,N-dimethyl-formamide;
DOI:10.1080/07328303.2012.689041