Li2Sn[PhB(μ-N-t-Bu)2]2

Base Information

• Chemical Name: Li2Sn[PhB(μ-N-t-Bu)2]2
• CAS No.: 1144563-01-8
• Molecular Formula: C₂₈H₄₆B₂Li₂N₄Sn
• Molecular Weight: 592.914
• Mol file: 1144563-01-8.mol

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Chemical Property of Li2Sn[PhB(μ-N-t-Bu)2]2

Chemical Property:

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Technology Process of Li2Sn[PhB(μ-N-t-Bu)2]2

There total 1 articles about Li2Sn[PhB(μ-N-t-Bu)2]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

tin(ll) chloride + bis(tert-butylamino)phenylborane dilithium salt (124652-56-8) → Li2Sn[PhB(μ-N-t-Bu)2]2 (1144563-01-8)

Guidance literature:

In diethyl ether; byproducts: LiCl; (N2, Schlenk) a soln. of Li-compound in diethyl ether was added to a suspn. of SnCl2 in diethyl ether at -80°C, the mixt. was stirred for30 min at -80°C and 5 h at 23°C; LiCl was filtered, the solvent was evapd. under vac., ppt. was washed with cold n-hexane; elem. anal.;

DOI:10.1139/V08-183

upstream raw materials:

bis(tert-butylamino)phenylborane dilithium salt