Technology Process of C29H23BrN2O4
There total 1 articles about C29H23BrN2O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
1,1,1,3,3,3-hexachloro-propan-2-one; triphenylphosphine;
In
dichloromethane;
at -10 - 20 ℃;
for 0.583333h;
DOI:10.1016/j.bmcl.2012.11.011
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrakis(triphenylphosphine) palladium(0) / toluene / 1 h / Reflux
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 °C
3: ethanol / 24 h / Reflux
With
tetrakis(triphenylphosphine) palladium(0); 3-chloro-benzenecarboperoxoic acid;
In
ethanol; dichloromethane; toluene;
DOI:10.1016/j.bmcl.2012.11.011
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetrakis(triphenylphosphine) palladium(0) / toluene / 1 h / Reflux
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 °C
3: ethanol / 24 h / Reflux
4: palladium 10% on activated carbon; cyclohexa-1,4-diene / ethanol / 24 h / Reflux
With
tetrakis(triphenylphosphine) palladium(0); cyclohexa-1,4-diene; palladium 10% on activated carbon; 3-chloro-benzenecarboperoxoic acid;
In
ethanol; dichloromethane; toluene;
DOI:10.1016/j.bmcl.2012.11.011