[Pd2(μ-3,5-dimethylpyrazole(-H))2(3,5-dimethylpyrazole)2(p-hydroxybenzoate-κO)2]

Base Information

Chemical Name:[Pd2(μ-3,5-dimethylpyrazole(-H))2(3,5-dimethylpyrazole)2(p-hydroxybenzoate-κO)2]
CAS No.:916852-88-5
Molecular Formula:C₃₄H₄₀N₈O₆Pd₂
Molecular Weight:869.582
Hs Code.:

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Chemical Property of [Pd2(μ-3,5-dimethylpyrazole(-H))2(3,5-dimethylpyrazole)2(p-hydroxybenzoate-κO)2]

Chemical Property:

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Technology Process of [Pd2(μ-3,5-dimethylpyrazole(-H))2(3,5-dimethylpyrazole)2(p-hydroxybenzoate-κO)2]

There total 1 articles about [Pd2(μ-3,5-dimethylpyrazole(-H))2(3,5-dimethylpyrazole)2(p-hydroxybenzoate-κO)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 609341-85-7
[Pd2(μ-3.5-dimethylpyrazole(-H))2(3,5-dimethylpyrazole(-H))2(3,5-dimethylpyrazole)2]

: 99-96-7
4-hydroxy-benzoic acid

: 916852-88-5
[Pd2(μ-3,5-dimethylpyrazole(-H))2(3,5-dimethylpyrazole)2(p-hydroxybenzoate-κO)2]

Guidance literature:: In methanol; dichloromethane; byproducts: 3,5-dimethylpyrazole; methanolic soln. of ligand (0.539 mmol) added to soln. of Pd compd. (0.269 mmol) in CH2Cl2, stirred at room temp. for 2 h; evapd., triturated (Et2O), elem. anal.;
DOI:10.1002/ejic.200500791

Reference yield: 38.0%

: 916852-88-5
[Pd2(μ-3,5-dimethylpyrazole(-H))2(3,5-dimethylpyrazole)2(p-hydroxybenzoate-κO)2]

: silver perchlorate

: [Pd2Ag2(μ-3,5-dimethylpyrazole(-H))4(p-hydroxybenzoate-κO)2]

Guidance literature:: With Et₃N; In acetone; byproducts: Et3NHClO4; AgClO4 (0.392 mmol) and Et3N (0.75 ml) added to soln. of Pd compd. (0.196 mmol) in acetone, stirred at room temp. for 75 min; filtered (celite), evapd., triturated (MeOH), washed (Et2O), elem. anal.;
DOI:10.1002/ejic.200500791

Reference yield:

: 916852-88-5
[Pd2(μ-3,5-dimethylpyrazole(-H))2(3,5-dimethylpyrazole)2(p-hydroxybenzoate-κO)2]

: [Pd₂Ag₂(C₃HN₂(CH₃)2)4(O₂CC₆H₄OH)2]

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / acetone

2: acetone

With Et₃N; In acetone;
DOI:10.1002/ejic.200500791