C₃₉H₄₇ClN₂O₁₀

Base Information

Chemical Name:C₃₉H₄₇ClN₂O₁₀
CAS No.:1424402-60-7
Molecular Formula:C₃₉H₄₇ClN₂O₁₀
Molecular Weight:739.263
Hs Code.:

C<sub>39</sub>H<sub>47</sub>ClN<sub>2</sub>O<sub>10</sub>

Synonyms:

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Chemical Property of C₃₉H₄₇ClN₂O₁₀

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Technology Process of C₃₉H₄₇ClN₂O₁₀

There total 20 articles about C₃₉H₄₇ClN₂O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₀H₄₈BrClN₂O₁₁

: 1424402-60-7
C₃₉H₄₇ClN₂O₁₀

Guidance literature:: With potassium carbonate; In 1,2-dimethoxyethane; ethylene glycol; at 20 ℃; for 0.05h; Inert atmosphere;
DOI:10.1021/jm301346z

Reference yield:

: 1424401-73-9
4-((R)-4-benzyl-2-oxooxazolidine-3-yl)-4-butyric acid allyl ester

: 1424402-60-7
C₃₉H₄₇ClN₂O₁₀

Guidance literature:: Multi-step reaction with 13 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: 0.5 h / 20 °C / Inert atmosphere

2.1: trifluoroacetic acid / tetrahydrofuran; dichloromethane / 16 h / 20 °C / Inert atmosphere

3.1: triethylamine; chloroformic acid ethyl ester / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

3.2: 1 h / 0 °C / Inert atmosphere

4.1: 16 h / Reflux; Inert atmosphere

5.1: dihydrogen peroxide; lithium hydroxide monohydrate / tetrahydrofuran; water / 0.67 h / 0 °C / Inert atmosphere

6.1: trifluoroacetic acid / dichloromethane / 16 h / 20 °C / Inert atmosphere

7.1: sodium hydrogencarbonate / water; acetone / 4 h / 20 °C / Inert atmosphere

8.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C / Inert atmosphere

9.1: piperidine / N,N-dimethyl-formamide / 16 h / 20 °C / Inert atmosphere

10.1: trifluoroacetic acid / dichloromethane; water / 3 h / 0 °C / Inert atmosphere

11.1: pyridinium p-toluenesulfonate / dichloromethane / 2 h / 20 °C / Inert atmosphere

12.1: Acetyl bromide / dichloromethane / 4 h / 20 °C / Inert atmosphere

13.1: potassium carbonate / ethylene glycol; 1,2-dimethoxyethane / 0.05 h / 20 °C / Inert atmosphere

With piperidine; dmap; lithium hydroxide monohydrate; Acetyl bromide; dihydrogen peroxide; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; chloroformic acid ethyl ester; sodium hydrogencarbonate; potassium carbonate; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water; ethylene glycol; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jm301346z

Reference yield:

: 350245-09-9
2-(tert-butyl-dimethyl-silanyloxy)-4-methyl-pentanoyl chloride

: 1424402-60-7
C₃₉H₄₇ClN₂O₁₀

Guidance literature:: Multi-step reaction with 8 steps

1: dmap; triethylamine / dichloromethane / 1 h / 20 °C / Cooling with ice; Inert atmosphere

2: ammonium cerium (IV) nitrate / methanol / 17 h / 0 °C / Inert atmosphere

3: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C / Inert atmosphere

4: piperidine / N,N-dimethyl-formamide / 16 h / 20 °C / Inert atmosphere

5: trifluoroacetic acid / dichloromethane; water / 3 h / 0 °C / Inert atmosphere

6: pyridinium p-toluenesulfonate / dichloromethane / 2 h / 20 °C / Inert atmosphere

7: Acetyl bromide / dichloromethane / 4 h / 20 °C / Inert atmosphere

8: potassium carbonate / ethylene glycol; 1,2-dimethoxyethane / 0.05 h / 20 °C / Inert atmosphere

With piperidine; dmap; ammonium cerium (IV) nitrate; Acetyl bromide; pyridinium p-toluenesulfonate; potassium carbonate; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In methanol; 1,2-dimethoxyethane; dichloromethane; water; ethylene glycol; N,N-dimethyl-formamide;
DOI:10.1021/jm301346z